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MassMS-NW-6661 diethylene glycol bis(2-chloroethyl) ether C8H16Cl2O3 (Mass of molecular ion: 230)
Source Temperature: 260 °C Sample Temperature: 190 °C Reservoir, 75 eV
15.0 3.2 19.0 1.1 26.0 1.6 27.0 29.9 28.0 8.2 29.0 5.1 31.0 6.3 36.0 1.0 43.0 16.9 44.0 4.9 45.0 56.6 46.0 1.4 49.0 1.8 51.0 3.3 57.0 1.5 58.0 1.4 59.0 16.4 62.0 2.8 63.0 100.0 64.0 3.3 65.0 30.7 70.0 1.5 71.0 1.2 72.0 3.1 73.0 8.0 87.0 3.4 93.0 6.2 95.0 2.2 101.0 2.9 103.0 1.0 105.0 1.1 106.0 17.7 107.0 51.1 108.0 8.0 109.0 16.3 115.0 1.5 137.0 16.5 138.0 1.1 139.0 5.8 151.0 1.9
90 MHz in CDCl3
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1H NMR 89.56 MHz C8 H16 Cl2 O3 0.05 ml : 0.5 ml CDCl3 diethylene glycol bis(2-chloroethyl) ether 
Assign. Shift(ppm)
A 3.78 B 3.68 C 3.62
Hz ppm Int.345.25 3.855 27 342.06 3.820 50 340.38 3.801 23 340.06 3.798 23 337.00 3.763 149 333.31 3.722 186 332.69 3.715 198 329.50 3.680 1000 325.69 3.637 170 320.63 3.581 60 317.44 3.545 34
in CDCl3
liquid film
4880 A,200 M,liquid
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