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MassMS-IW-0913 2-(2-(2-chloroethoxy)ethoxy)ethanol C6H13ClO3 (Mass of molecular ion: 168)
Source Temperature: 220 °C Sample Temperature: 150 °C Reservoir, 75 eV
15.0 1.4 19.0 2.7 27.0 16.0 28.0 6.6 29.0 3.5 31.0 8.5 43.0 11.7 44.0 12.1 45.0 100.0 46.0 3.2 57.0 1.2 58.0 24.1 59.0 15.5 62.0 1.6 63.0 57.0 64.0 1.7 65.0 18.1 72.0 1.0 73.0 3.9 75.0 33.4 76.0 1.3 87.0 5.3 88.0 3.7 89.0 18.2 93.0 7.8 95.0 2.6 101.0 3.1 102.0 2.5 106.0 6.2 107.0 26.5 108.0 3.2 109.0 8.5 137.0 7.2 139.0 2.3
400 MHz in CDCl3
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1H NMR 399.65 MHz C6 H13 Cl O3 0.05 ml : 0.5 ml CDCl3 2-(2-(2-chloroethoxy)ethoxy)ethanol 
Assign. Shift(ppm)
A 3.766 B 3.730 C 3.69 D 3.653 E 3.612 F 3.09 ASSIGNED BY C-H COSY
Hz ppm Int.1512.21 3.784 226 1511.47 3.782 227 1506.47 3.770 453 1505.49 3.768 295 1500.61 3.755 372 1500.12 3.754 358 1495.97 3.744 239 1493.65 3.738 116 1491.70 3.733 311 1490.11 3.729 190 1488.53 3.725 118 1486.69 3.720 335 1483.52 3.713 56 1482.30 3.709 46 1480.10 3.704 100 1478.88 3.701 153 1478.03 3.699 174 1474.00 3.689 1000 1469.48 3.677 160 1467.41 3.672 113 1465.33 3.667 380 1464.84 3.666 381 1459.96 3.654 299 1459.23 3.652 437 1456.30 3.644 49 1455.20 3.642 54 1453.86 3.638 230 1453.13 3.637 228 1447.88 3.623 399 1446.04 3.619 113 1444.46 3.615 194 1442.99 3.611 325 1440.92 3.606 102 1438.60 3.600 251 1234.50 3.089 57
in CDCl3
liquid film
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