-
MassMS-KW-0551 N-benzyloxycarbonyl-L-phenylalaninol C17H19NO3 (Mass of molecular ion: 271)
Source Temperature: 150 °C Sample Temperature: 130 °C Direct, 75 eV
15.0 3.6 18.0 2.9 27.0 4.4 28.0 3.9 29.0 2.8 30.0 1.2 31.0 1.5 37.0 1.0 38.0 2.4 39.0 11.3 40.0 1.1 41.0 2.7 42.0 31.8 43.0 8.4 44.0 2.1 50.0 7.5 51.0 17.7 52.0 4.9 53.0 4.2 53.5 1.3 54.0 1.2 55.0 1.0 58.0 7.1 62.0 2.4 63.0 6.7 64.0 1.8 65.0 17.1 66.0 1.4 74.0 2.5 75.0 1.8 76.0 1.7 77.0 33.3 78.0 12.6 79.0 50.8 80.0 5.1 85.0 3.9 86.0 70.9 87.0 3.1 89.0 6.4 90.0 6.3 91.0 99.1 92.0 100.0 93.0 7.7 103.0 3.8 104.0 2.8 105.0 10.8 106.0 4.6 107.0 35.1 108.0 43.6 109.0 3.4 115.0 4.3 116.0 3.4 117.0 2.4 118.0 1.4 131.0 1.1 132.0 1.1 133.0 1.9 134.0 9.5 135.0 1.0 150.0 3.2 177.0 6.5 178.0 1.1 194.0 2.7
400 MHz in CDCl3
-
1H NMR 399.65 MHz C17H19NO3 0.040 g : 0.5 ml CDCl3 N-benzyloxycarbonyl-L-phenylalaninol 
Assign. Shift(ppm)
A 7.30 B 7.19 C 5.20 D 5.039 E 3.922 F *1 3.61 G *1 3.53 J 2.823 K 2.78
Hz ppm Int.2935.43 7.343 95 2932.74 7.336 139 2927.01 7.322 325 2925.66 7.319 276 2923.47 7.313 262 2919.80 7.304 793 2917.97 7.299 529 2916.39 7.295 427 2911.99 7.284 631 2903.20 7.262 519 2895.88 7.244 338 2890.39 7.230 196 2884.89 7.217 221 2877.81 7.199 286 2871.95 7.184 314 2865.73 7.169 214 2076.91 5.196 80 2026.49 5.069 40 2014.04 5.038 1000 2000.86 5.005 25 1567.88 3.922 78 1442.02 3.608 104 1409.31 3.526 86 1131.96 2.832 236 1125.13 2.815 246 1109.01 2.775 120
in CDCl3
KBr disk
Nujol
更多供应商
