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MassMS-NW-6201 L-2-amino-3-phenyl-1-propanol C9H13NO (Mass of molecular ion: 151)
Source Temperature: 260 °C Sample Temperature: 190 °C Reservoir, 75 eV
15.0 1.6 18.0 1.4 28.0 3.3 30.0 3.6 31.0 1.3 39.0 3.0 41.0 1.4 42.0 14.7 43.0 1.9 50.0 1.0 51.0 2.5 59.0 1.2 59.5 1.2 60.0 100.0 61.0 2.7 63.0 1.6 65.0 4.4 77.0 5.1 78.0 1.2 89.0 1.1 91.0 12.7 92.0 3.1 93.0 1.9 103.0 7.4 104.0 1.5 117.0 1.3 118.0 1.9 119.0 1.3 120.0 33.0 121.0 3.2
400 MHz in CDCl3
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1H NMR 399.65 MHz C9 H13 N O 0.039 g : 0.5 ml CDCl3 L-2-amino-3-phenyl-1-propanol 
Assign. Shift(ppm)
A 7.287 B 7.20 C 7.19 D *1 3.591 E *1 3.374 F 3.093 G *2 2.777 J *2 2.513 K 2.4 J(D,E)=-10.6HZ J(D,F)=4.0HZ J(E,F)=7.2HZ J(F,G)=5.3HZ J(F,J)=8.5HZ J(G,J)=-13.4HZ
Hz ppm Int.2922.12 7.312 236 2921.14 7.310 343 2919.56 7.306 182 2915.89 7.297 318 2914.06 7.292 864 2910.64 7.283 131 2908.08 7.277 351 2906.74 7.274 775 2888.92 7.229 173 2887.57 7.226 354 2886.23 7.222 323 2878.91 7.204 1000 2877.44 7.200 975 2875.12 7.195 229 2874.39 7.193 225 2870.73 7.184 735 1443.24 3.612 381 1439.21 3.602 401 1432.62 3.585 487 1428.59 3.575 473 1357.18 3.396 426 1349.98 3.378 488 1346.44 3.370 353 1339.36 3.352 392 1248.41 3.124 105 1244.38 3.114 125 1243.16 3.111 147 1241.21 3.106 139 1239.75 3.103 188 1239.26 3.101 188 1237.30 3.096 143 1235.96 3.093 259 1234.62 3.090 171 1232.67 3.085 178 1230.71 3.080 155 1228.76 3.075 133 1227.54 3.072 134 1223.51 3.062 103 1120.12 2.803 260 1114.87 2.790 246 1106.69 2.770 336 1101.44 2.757 305 1015.01 2.540 374 1006.47 2.519 367 1001.59 2.507 322 993.04 2.485 306
in CDCl3
KBr disc
nujol mull
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