4-甲基苯肼盐酸盐

Mass

MS-NW-0632          
p-tolylhydrazine hydrochloride
C7H10N2 HCl         (Mass of molecular ion:    122)

   Source Temperature: 200 °C
   Sample Temperature: 160 °C
   Direct, 75 eV

      17.0       1.3
      18.0       5.2
      26.0       1.2
      27.0       5.3
      28.0       4.2
      29.0       3.2
      31.0       1.6
      35.0       5.7
      36.0      32.8
      37.0       1.9
      38.0      10.4
      39.0      12.0
      40.0       1.5
      41.0       3.4
      43.0       1.2
      50.0       6.1
      51.0      12.5
      52.0       8.1
      53.0       5.1
      54.0       1.1
      61.0       1.2
      62.0       2.6
      63.0       6.3
      64.0       2.3
      65.0      12.7
      66.0       1.8
      67.0       1.2
      74.0       1.0
      75.0       1.0
      76.0       1.6
      77.0      36.1
      78.0      16.6
      79.0      40.0
      80.0       3.6
      89.0       3.1
      90.0       1.8
      91.0      24.5
      92.0       9.4
      93.0       3.5
      94.0       1.6
     104.0       8.9
     105.0       7.1
     106.0      56.9
     107.0      12.5
     120.0       2.1
     121.0       9.4
     122.0     100.0
     123.0       8.5

Assign. Shift(ppm) A 7.26 B 7.04 C 4.83 D 2.311 C-PEAK INCLUDES H2O.

     Hz     ppm     Int.

    656.19   7.327     75
    655.81   7.323     76
    647.56   7.231    159
    635.50   7.096     49
    633.25   7.071    202
    631.06   7.047     57
    626.69   6.998     47
    624.63   6.975     93
    432.31   4.828   1000
    207.00   2.312    444