3-甲基苯肼盐酸盐

产品名称 3-甲基苯肼盐酸盐

CAS号637-04-7

分子式C7H11ClN2

分子量158.63

¹³CNMR

Mass

MS-NW-0640          
m-tolylhydrazine hydrochloride
C7H10N2 HCl         (Mass of molecular ion:    122)

   Source Temperature: 190 °C
   Sample Temperature: 150 °C
   Direct, 75 eV

      18.0       1.2
      27.0       3.3
      28.0       2.7
      29.0       2.3
      31.0       1.3
      35.0       3.9
      36.0      29.4
      37.0       1.3
      38.0       9.6
      39.0      10.8
      40.0       1.3
      41.0       2.7
      50.0       3.7
      51.0       8.0
      52.0       4.8
      53.0       3.4
      60.0       1.9
      61.0       1.9
      62.0       1.9
      63.0       5.2
      64.0       2.1
      65.0      11.4
      66.0       1.7
      67.0       1.1
      76.0       1.2
      77.0      29.5
      78.0      13.8
      79.0      33.2
      80.0       3.7
      89.0       2.6
      90.0       1.3
      91.0      21.3
      92.0      12.7
      93.0       4.9
      94.0       2.5
     104.0      10.3
     105.0       5.4
     106.0      34.6
     107.0      10.0
     121.0       4.4
     122.0     100.0
     123.0       8.4

90 MHz in D2O

¹H NMR	89.56 MHz
C₇ H₁₀ N₂	saturated in D₂O
m-tolylhydrazine hydrochloride

    Assign.     Shift(ppm)

      A             7.32
      B             7.01
      C             6.92
      D             6.90
      E             2.346
     
     SOLVENT PEAK REMOVED

     Hz     ppm     Int.

    664.94   7.425     60
    657.50   7.342    116
    650.38   7.262     79
    648.63   7.243    139
    631.19   7.048    158
    620.00   6.923    382
    613.19   6.847    102
    210.25   2.348   1000

in D2O

KBr disc

nujol mull

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