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二乙基汞

产品名称 二乙基汞

CAS号627-44-1

分子式C4H10Hg

分子量258.71

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  • Mass

    MS-NW-3721          
    diethylmercury
    C4H10Hg             (Mass of molecular ion:    260)
    

       Source Temperature: 280 °C
       Sample Temperature: 180 °C
       Reservoir, 75 eV
    

          26.0       3.8
          27.0      21.4
          28.0       9.7
          29.0     100.0
          30.0       2.2
          41.0       1.2
          43.0       2.3
          58.0       1.8
         199.0       1.7
         200.0       2.4
         201.0       1.6
         202.0       3.0
         227.0       2.1
         228.0       3.6
         229.0       4.7
         230.0       3.3
         231.0       5.4
         233.0       1.2
         256.0       1.7
         257.0       3.0
         258.0       4.1
         259.0       2.5
         260.0       5.2
         262.0       1.1
    

400 MHz in CDCl3

90 MHz in CDCl3


  • 1H NMR 399.65 MHz
    C4 H10 Hg 0.05 ml : 0.5 ml CDCl3
    diethylmercury
    ChemicalStructure
        Assign.     Shift(ppm)
    A 1.289 B 1.003 SATELLITE PEAKS EXIST.

         Hz     ppm     Int.
    

        587.28   1.470     40
        579.35   1.450     72
        571.29   1.430     41
        542.97   1.359     31
        536.87   1.344     64
        535.03   1.339     45
        529.05   1.324    132
        528.56   1.323    146
        524.17   1.312    539
        520.87   1.304    118
        516.48   1.293    919
        515.99   1.292   1000
        508.18   1.272    596
        491.94   1.231     33
        451.54   1.130    182
        413.09   1.034    260
        405.27   1.015    618
        397.22   0.994    536
        388.92   0.974    157
        356.69   0.893     37
        348.63   0.873     34
    


  • 1H NMR 89.56 MHz
    C4 H10 Hg 0.04 ml : 0.5 ml CDCl3
    diethylmercury
    ChemicalStructure
        Assign.     Shift(ppm)
    A 1.28 B 0.99

         Hz     ppm     Int.
    

        186.75   2.086     31
        178.63   1.995     88
        170.88   1.908     39
        134.56   1.503     36
        128.19   1.432     31
        127.19   1.421     91
        124.38   1.389     80
        123.63   1.381    118
        121.81   1.361    119
        120.88   1.350    114
        118.19   1.320     89
        117.81   1.316     89
        115.31   1.288   1000
        113.63   1.269     37
        113.06   1.263     38
        112.31   1.255     32
        110.25   1.232    297
        109.44   1.222    352
        108.69   1.214    312
        107.94   1.206    346
         99.81   1.115    208
         98.00   1.095    170
         93.31   1.042    314
         92.75   1.036    289
         91.75   1.025    105
         86.13   0.962    140
         84.31   0.942    159
         80.19   0.896     42
         78.13   0.873     40
         74.69   0.834     30
         59.63   0.666     37
         52.00   0.581     82
         45.00   0.503     40
         43.75   0.489     31
         37.06   0.414     33
    

in CDCl3



liquid film



GAMMA-RAY IRRAD. IN SI(CH3)4 AT 77K, CENTRAL PART

ANION RADICAL, GAMMA-RAY IRRAD. IN SI(CH3)4 AT 77K





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