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MassMS-NW-3721 diethylmercury C4H10Hg (Mass of molecular ion: 260)
Source Temperature: 280 °C Sample Temperature: 180 °C Reservoir, 75 eV
26.0 3.8 27.0 21.4 28.0 9.7 29.0 100.0 30.0 2.2 41.0 1.2 43.0 2.3 58.0 1.8 199.0 1.7 200.0 2.4 201.0 1.6 202.0 3.0 227.0 2.1 228.0 3.6 229.0 4.7 230.0 3.3 231.0 5.4 233.0 1.2 256.0 1.7 257.0 3.0 258.0 4.1 259.0 2.5 260.0 5.2 262.0 1.1
400 MHz in CDCl3
90 MHz in CDCl3
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1H NMR 399.65 MHz C4 H10 Hg 0.05 ml : 0.5 ml CDCl3 diethylmercury 
Assign. Shift(ppm)
A 1.289 B 1.003 SATELLITE PEAKS EXIST.
Hz ppm Int.587.28 1.470 40 579.35 1.450 72 571.29 1.430 41 542.97 1.359 31 536.87 1.344 64 535.03 1.339 45 529.05 1.324 132 528.56 1.323 146 524.17 1.312 539 520.87 1.304 118 516.48 1.293 919 515.99 1.292 1000 508.18 1.272 596 491.94 1.231 33 451.54 1.130 182 413.09 1.034 260 405.27 1.015 618 397.22 0.994 536 388.92 0.974 157 356.69 0.893 37 348.63 0.873 34
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1H NMR 89.56 MHz C4 H10 Hg 0.04 ml : 0.5 ml CDCl3 diethylmercury Assign. Shift(ppm)
A 1.28 B 0.99
Hz ppm Int.186.75 2.086 31 178.63 1.995 88 170.88 1.908 39 134.56 1.503 36 128.19 1.432 31 127.19 1.421 91 124.38 1.389 80 123.63 1.381 118 121.81 1.361 119 120.88 1.350 114 118.19 1.320 89 117.81 1.316 89 115.31 1.288 1000 113.63 1.269 37 113.06 1.263 38 112.31 1.255 32 110.25 1.232 297 109.44 1.222 352 108.69 1.214 312 107.94 1.206 346 99.81 1.115 208 98.00 1.095 170 93.31 1.042 314 92.75 1.036 289 91.75 1.025 105 86.13 0.962 140 84.31 0.942 159 80.19 0.896 42 78.13 0.873 40 74.69 0.834 30 59.63 0.666 37 52.00 0.581 82 45.00 0.503 40 43.75 0.489 31 37.06 0.414 33
in CDCl3
liquid film
GAMMA-RAY IRRAD. IN SI(CH3)4 AT 77K, CENTRAL PART
ANION RADICAL, GAMMA-RAY IRRAD. IN SI(CH3)4 AT 77K
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