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3,4,4'-三氨基二苯醚

产品名称 3,4,4'-三氨基二苯醚

CAS号6264-66-0

分子式C12H13N3O

分子量215.25

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  • Mass

    MS-IW-7600          
    4-(4-aminophenoxy)-o-phenylenediamine
    C12H13N3O           (Mass of molecular ion:    215)
    

       Source Temperature: 170 °C
       Sample Temperature: 180 °C
       Direct, 75 eV
    

          27.0       1.4
          28.0       2.6
          39.0       2.2
          41.0       1.3
          51.0       1.4
          52.0       3.3
          53.0       3.8
          54.0       1.6
          63.0       1.7
          65.0       3.8
          66.0       1.3
          78.0       2.0
          79.0       2.1
          80.0       8.1
          81.0       1.3
          90.0       2.1
          91.0       1.1
          92.0       1.2
          93.0       3.7
          94.0       1.1
          95.0       4.9
          96.0       1.1
          99.0       1.6
         105.0       1.0
         106.0       2.8
         107.0       2.8
         107.5       3.4
         108.0      13.3
         109.0       3.7
         123.0       7.9
         124.0       1.2
         143.0       1.5
         159.0       1.1
         169.0       4.4
         170.0       8.9
         171.0       4.6
         186.0       6.6
         187.0       2.4
         197.0       3.5
         198.0       1.1
         214.0       4.3
         215.0     100.0
         216.0      14.2
         217.0       1.2
    

400 MHz in DMSO-d6


  • 1H NMR 399.65 MHz
    C12 H13 N3 O 0.040 g : 0.5 ml DMSO-d6
    4-(4-aminophenoxy)-o-phenylenediamine
    ChemicalStructure
        Assign.     Shift(ppm)
    A 6.640 B 6.520 C 6.433 D 6.159 E 5.984 F *1 4.75 G *1 4.55 J *1 4.14

         Hz     ppm     Int.
    

       2661.99   6.661     88
       2658.69   6.653    699
       2656.62   6.648    283
       2652.10   6.637    342
       2649.90   6.631   1000
       2646.73   6.623    149
       2612.92   6.539    143
       2609.74   6.531    993
       2607.54   6.525    333
       2603.03   6.514    292
       2600.95   6.509    708
       2597.66   6.500    100
       2575.32   6.444    530
       2567.02   6.424    584
       2463.01   6.163    586
       2460.33   6.157    619
       2397.09   5.998    339
       2394.41   5.992    317
       2388.92   5.978    317
       2386.11   5.971    297
       1899.66   4.754    332
       1817.63   4.549    472
       1655.76   4.144    284
    

in DMSO-d6



KBr disc



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