-
MassMS-NW-9477 3,4'-oxydianiline C12H12N2O (Mass of molecular ion: 200)
Source Temperature: 170 °C Sample Temperature: 120 °C Direct, 75 eV
17.0 1.0 18.0 5.0 28.0 1.5 39.0 4.5 41.0 1.2 52.0 2.2 53.0 3.0 54.0 1.2 63.0 1.9 64.0 1.9 65.0 11.8 66.0 2.6 80.0 9.8 81.0 1.1 86.0 2.6 91.0 1.3 92.0 3.6 93.0 9.9 99.5 1.0 100.0 6.2 106.0 1.3 108.0 27.6 109.0 5.8 117.0 1.3 127.0 1.3 130.0 2.1 131.0 1.6 143.0 1.0 144.0 2.8 145.0 1.7 154.0 3.1 155.0 2.3 156.0 4.7 157.0 1.0 171.0 16.3 172.0 17.2 173.0 2.1 182.0 2.2 183.0 2.9 198.0 1.0 199.0 6.7 200.0 100.0 201.0 14.1 202.0 1.1
400 MHz in CDCl3
-
1H NMR 399.65 MHz C12 H12 N2 O 0.034 g : 0.5 ml CDCl3 3,4'-oxydianiline 
Assign. Shift(ppm)
A 7.027 B 6.857 C 6.642 D 6.32 E 6.226 F 3.60
Hz ppm Int.2816.77 7.049 275 2808.72 7.028 563 2800.66 7.008 311 2749.15 6.879 80 2745.73 6.871 759 2743.41 6.865 279 2739.14 6.854 305 2736.82 6.849 1000 2733.52 6.840 121 2662.35 6.662 113 2658.94 6.654 940 2656.62 6.648 320 2654.30 6.642 54 2652.34 6.637 285 2650.02 6.631 823 2646.73 6.623 91 2530.88 6.333 150 2530.03 6.331 345 2529.05 6.329 389 2527.83 6.326 437 2526.73 6.323 374 2525.88 6.321 188 2522.83 6.313 169 2521.97 6.311 302 2520.87 6.308 377 2519.90 6.306 424 2518.68 6.303 336 2517.82 6.301 193 2490.60 6.232 350 2488.40 6.227 567 2486.21 6.221 282 1436.77 3.596 286
in CDCl3
KBr disc
nujol mull
更多供应商
