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MassMS-NW-2895 1,2-dichloroethyl ethyl ether C4H8Cl2O (Mass of molecular ion: 142)
Source Temperature: 210 °C Sample Temperature: 180 °C Reservoir, 75 eV
14.0 3.3 15.0 8.9 18.0 1.3 26.0 7.1 27.0 36.7 28.0 5.5 29.0 100.0 30.0 2.1 31.0 11.4 35.0 1.8 36.0 15.4 38.0 5.1 41.0 2.7 42.0 13.9 43.0 19.0 44.0 5.1 45.0 11.9 47.0 5.2 48.0 1.9 49.0 7.0 50.0 4.1 51.0 2.3 52.0 1.1 59.0 2.8 61.0 6.6 63.0 2.7 65.0 10.0 67.0 3.3 72.0 1.1 75.0 2.9 76.0 1.0 77.0 1.0 78.0 70.7 79.0 33.8 80.0 23.0 81.0 10.5 93.0 39.7 94.0 1.5 95.0 12.4 97.0 3.4 99.0 2.3 103.0 3.9 106.0 24.1 107.0 20.2 108.0 8.4 109.0 6.1
90 MHz in CDCl3
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1H NMR 89.56 MHz C4 H8 Cl2 O 0.05 ml : 0.5 ml CDCl3 1,2-dichloroethyl ethyl ether 
Assign. Shift(ppm)
A 5.632 B *1 3.95 C 3.79 D *1 3.58 E 1.293
Hz ppm Int.510.19 5.697 166 505.06 5.640 203 504.19 5.630 174 499.06 5.573 187 366.00 4.087 85 363.69 4.061 56 358.88 4.008 92 356.50 3.981 174 351.75 3.928 42 349.38 3.902 162 345.13 3.854 385 344.13 3.843 394 342.31 3.823 94 341.31 3.811 72 339.06 3.786 723 334.25 3.733 160 332.50 3.713 51 327.25 3.654 170 324.69 3.626 93 320.44 3.578 79 317.69 3.548 93 316.44 3.534 39 310.81 3.471 57 122.63 1.370 506 115.63 1.292 1000 108.50 1.212 446
in CDCl3
liquid film
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