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1,2-二氯乙氧基乙烷

产品名称 1,2-二氯乙氧基乙烷

CAS号623-46-1

分子式C4H8Cl2O

分子量143.01

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  • Mass

    MS-NW-2895          
    1,2-dichloroethyl ethyl ether
    C4H8Cl2O            (Mass of molecular ion:    142)
    

       Source Temperature: 210 °C
       Sample Temperature: 180 °C
       Reservoir, 75 eV
    

          14.0       3.3
          15.0       8.9
          18.0       1.3
          26.0       7.1
          27.0      36.7
          28.0       5.5
          29.0     100.0
          30.0       2.1
          31.0      11.4
          35.0       1.8
          36.0      15.4
          38.0       5.1
          41.0       2.7
          42.0      13.9
          43.0      19.0
          44.0       5.1
          45.0      11.9
          47.0       5.2
          48.0       1.9
          49.0       7.0
          50.0       4.1
          51.0       2.3
          52.0       1.1
          59.0       2.8
          61.0       6.6
          63.0       2.7
          65.0      10.0
          67.0       3.3
          72.0       1.1
          75.0       2.9
          76.0       1.0
          77.0       1.0
          78.0      70.7
          79.0      33.8
          80.0      23.0
          81.0      10.5
          93.0      39.7
          94.0       1.5
          95.0      12.4
          97.0       3.4
          99.0       2.3
         103.0       3.9
         106.0      24.1
         107.0      20.2
         108.0       8.4
         109.0       6.1
    

90 MHz in CDCl3


  • 1H NMR 89.56 MHz
    C4 H8 Cl2 O 0.05 ml : 0.5 ml CDCl3
    1,2-dichloroethyl ethyl ether
    ChemicalStructure
        Assign.     Shift(ppm)
    A 5.632 B *1 3.95 C 3.79 D *1 3.58 E 1.293

         Hz     ppm     Int.
    

        510.19   5.697    166
        505.06   5.640    203
        504.19   5.630    174
        499.06   5.573    187
        366.00   4.087     85
        363.69   4.061     56
        358.88   4.008     92
        356.50   3.981    174
        351.75   3.928     42
        349.38   3.902    162
        345.13   3.854    385
        344.13   3.843    394
        342.31   3.823     94
        341.31   3.811     72
        339.06   3.786    723
        334.25   3.733    160
        332.50   3.713     51
        327.25   3.654    170
        324.69   3.626     93
        320.44   3.578     79
        317.69   3.548     93
        316.44   3.534     39
        310.81   3.471     57
        122.63   1.370    506
        115.63   1.292   1000
        108.50   1.212    446
    

in CDCl3



liquid film