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MassMS2004-02551WA azidobenzene C6H5N3 (Mass of molecular ion: 119)
Source Temperature: 220 °C Sample Temperature: 150 °C Reservoir, 70 eV
26.0 2.6 27.0 5.8 28.0 8.8 31.0 1.5 37.0 10.3 37.5 2.1 38.0 21.8 38.5 3.7 39.0 21.8 40.0 5.7 41.0 14.4 43.0 1.9 44.0 1.1 44.5 3.7 45.0 1.3 45.5 6.9 46.0 1.6 49.0 2.1 50.0 9.7 51.0 14.4 52.0 10.9 61.0 4.4 62.0 7.1 63.0 37.3 64.0 82.0 65.0 19.4 66.0 2.0 74.0 1.9 75.0 1.1 76.0 1.3 77.0 3.6 90.0 3.9 91.0 100.0 92.0 7.5 93.0 4.0 119.0 48.8 120.0 3.9
400 MHz in CDCl3
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1H NMR 399.65 MHz C6H5N3 1.5 mg : 0.5 ml CDCl3 azidobenzene 
Assign. Shift(ppm)
A 7.344 B 7.136 C 7.025
Hz ppm Int.2946.42 7.371 101 2944.46 7.366 539 2943.49 7.363 244 2942.27 7.360 228 2939.09 7.352 148 2937.99 7.349 304 2937.02 7.347 884 2935.92 7.344 842 2933.84 7.339 153 2930.30 7.330 286 2929.20 7.327 330 2928.47 7.326 793 2926.27 7.320 114 2860.48 7.156 203 2859.38 7.153 387 2858.28 7.150 231 2853.40 7.138 225 2852.06 7.135 583 2851.20 7.132 273 2850.71 7.131 199 2845.59 7.118 149 2844.49 7.116 275 2843.39 7.113 153 2814.70 7.041 183 2814.09 7.040 201 2812.99 7.037 861 2811.89 7.034 1000 2811.16 7.032 523 2809.70 7.029 276 2806.28 7.020 293 2805.42 7.018 467 2804.33 7.015 897 2803.47 7.013 700 2803.23 7.012 689 2801.03 7.007 94
in CDCl3
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