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网站主页CAS数据库列表 20237-98-3更多图谱2,6-双-(4-叠氮苯亚甲基)环己酮(20237-98-3)质谱(MS)

2,6-双-(4-叠氮苯亚甲基)环己酮

产品名称 2,6-双-(4-叠氮苯亚甲基)环己酮

CAS号20237-98-3

分子式C20H16N6O

分子量356.38

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  • Mass

    MS-NW-7450          
    2,6-bis(p-azidobenzylidene)cyclohexanone
    C20H16N6O           (Mass of molecular ion:    356)
    

       Source Temperature: 200 °C
       Sample Temperature: 180 °C
       Direct, 75 eV
    

          14.0       3.5
          17.0       2.3
          18.0      11.3
          27.0       2.3
          28.0     100.0
          29.0       1.8
          39.0       4.7
          41.0       2.1
          50.0       2.3
          51.0       4.1
          52.0       1.7
          53.0       1.2
          62.0       1.0
          63.0       3.6
          64.0       3.4
          65.0       2.3
          66.0       1.0
          75.0       1.8
          76.0       2.5
          77.0       4.3
          78.0       1.6
          88.0       1.4
          89.0       2.5
          90.0       1.3
          91.0       2.5
          93.0       1.0
          94.5       1.1
         101.0       2.2
         102.0       3.5
         103.0       2.3
         104.0       1.0
         106.0       1.7
         108.5       1.4
         114.0       1.3
         115.0       5.5
         116.0       4.3
         117.0       1.5
         119.0       1.4
         127.0       1.6
         128.0       3.3
         129.0       2.0
         130.0       1.8
         140.0       2.3
         141.0       1.3
         142.0       1.6
         143.0       1.5
         151.0       1.0
         152.0       1.5
         153.0       1.4
         154.0       1.4
         155.0       1.8
         156.0       1.0
         165.0       1.2
         166.0       2.0
         167.0       1.7
         170.0       1.4
         178.0       1.6
         180.0       1.4
         181.0       1.5
         182.0       1.1
         190.0       1.6
         191.0       1.5
         192.0       1.3
         193.0       1.1
         194.0       1.5
         202.0       1.1
         203.0       1.8
         204.0       1.9
         205.0       1.2
         215.0       2.8
         216.0       3.1
         217.0       1.9
         218.0       2.1
         228.0       1.7
         229.0       1.8
         230.0       2.0
         231.0       1.3
         232.0       1.1
         242.0       1.7
         243.0       5.6
         244.0       3.8
         245.0       1.8
         246.0       1.5
         255.0       1.4
         256.0       1.2
         257.0       1.3
         270.0       1.0
         271.0       9.2
         272.0       6.2
         273.0       3.2
         274.0       5.1
         275.0       1.4
         276.0       1.6
         299.0       1.2
         300.0       4.2
         301.0       1.5
         304.0       1.5
         328.0       9.7
         329.0       2.5
         330.0       1.7
         356.0       1.9
    

400 MHz in CDCl3


  • 1H NMR 399.65 MHz
    C20 H16 N6 O 0.043 g : 0.5 ml CDCl3
    2,6-bis(p-azidobenzylidene)cyclohexanone
    ChemicalStructure
        Assign.     Shift(ppm)
    A 7.739 B 7.460 C 7.048 D 2.895 E 1.799

         Hz     ppm     Int.
    

       3093.14   7.740    441
       2988.40   7.478    126
       2985.96   7.472    714
       2979.25   7.455    286
       2977.66   7.451    769
       2972.66   7.439     45
       2823.36   7.065    154
       2820.92   7.059   1000
       2819.09   7.054    337
       2814.21   7.042    314
       2812.38   7.038    899
       2809.94   7.032    127
       1164.67   2.915    234
       1162.60   2.910    271
       1156.86   2.895    379
       1152.22   2.884    286
       1150.27   2.879    253
        731.45   1.831     61
        729.37   1.826     42
        729.00   1.825     42
        725.10   1.815    132
        718.99   1.800    206
        712.89   1.784    126
        709.11   1.775     42
        706.54   1.768     55
    

KBr disc



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