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网站主页CAS数据库列表 622-03-7更多图谱二苯基硫代卡巴肼(622-03-7)核磁图(1HNMR)

二苯基硫代卡巴肼

产品名称 二苯基硫代卡巴肼

CAS号622-03-7

分子式C13H14N4S

分子量258.34

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  • Mass

    MS-NW-2392          
    1,5-diphenylthiocarbonohydrazide
    C13H14N4S           (Mass of molecular ion:    258)
    

       Source Temperature: 230 °C
       Sample Temperature: 150 °C
       Direct, 75 eV
    

          17.0       1.9
          18.0       8.4
          26.5       3.0
          27.5       7.7
          29.0       1.0
          31.5       2.6
          33.5       1.0
          37.0       1.9
          38.0       4.2
          39.0      12.2
          40.0       3.0
          41.0       3.7
          42.0       4.5
          43.0       1.9
          46.5       2.8
          50.0       5.5
          51.0      12.4
          52.0       4.6
          53.0       1.7
          54.0       2.8
          58.5       6.0
          59.5      22.9
          60.5       1.7
          61.5       2.6
          62.5       3.7
          63.5       4.2
          65.0      20.0
          66.0      25.3
          67.0       3.0
          74.0       1.4
          75.0       1.2
          76.0       1.9
          77.0      34.0
          78.0      12.5
          79.0       1.8
          80.0       1.1
          91.0       4.7
          92.0      26.0
          93.0     100.0
          94.0       8.9
         105.0      11.2
         106.0       5.4
         107.0       6.4
         108.0       7.9
         109.0       1.2
         109.5       2.3
         118.0       2.0
         125.0       1.5
         131.0       1.9
         133.0       1.3
         135.0       1.2
         136.0       3.7
         150.0       5.9
         151.0       1.2
         167.0       7.9
         168.0       1.7
         169.0       2.0
         256.0       1.2
         298.0       1.1
    

400 MHz in DMSO-d6 (at 60.0C)


  • 1H NMR 399.65 MHz
    C13 H14 N4 S 0.038 g : 0.5 ml DMSO-d6 at 60C
    1,5-diphenylthiocarbonohydrazide
    ChemicalStructure
        Assign.     Shift(ppm)
    A *1 9.6 B *1 7.6 C 7.158 D 6.76 E 6.74

         Hz     ppm     Int.
    

       3841.40   9.612    104
       3053.44   7.641     38
       2874.91   7.194     63
       2868.96   7.179    375
       2861.18   7.160    709
       2853.55   7.141    454
       2843.48   7.115     33
       2843.02   7.114     31
       2842.25   7.112     31
       2841.64   7.111     32
       2840.88   7.109     30
       2840.27   7.107     32
       2839.66   7.106     30
       2709.81   6.781    280
       2701.57   6.760    592
       2698.52   6.753   1000
       2690.73   6.733    921
       2680.51   6.708     45
       2679.90   6.706     43
       2678.99   6.704     44
       2677.46   6.700     49
       2677.00   6.699     49
    

in DMSO-d6



KBr disc



nujol mull