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网站主页CAS数据库列表 621-01-2更多图谱1,3-二对甲苯基-2-硫脲(621-01-2)Raman光谱

1,3-二对甲苯基-2-硫脲

产品名称 1,3-二对甲苯基-2-硫脲

CAS号621-01-2

分子式C15H16N2S

分子量256.37

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  • Mass

    MS-NW-0214          
    1,3-di(p-tolyl)-2-thiourea
    C15H16N2S           (Mass of molecular ion:    256)
    

       Source Temperature: 200 °C
       Sample Temperature:   0 °C
       Direct, 75 eV
    

          18.0       1.8
          27.0       2.6
          28.0       1.6
          38.0       1.3
          39.0       8.7
          41.0       2.7
          45.0       2.0
          50.0       3.0
          51.0       6.1
          52.0       3.3
          53.0       3.2
          54.0       1.0
          62.0       1.6
          63.0       5.8
          64.0       2.0
          65.0      15.1
          66.0       1.5
          74.5       1.3
          75.0       1.0
          76.0       1.0
          77.0      11.5
          78.0       4.4
          79.0       8.0
          80.0       1.9
          89.0       5.7
          90.0       3.4
          91.0      35.9
          92.0       4.1
         104.0       3.4
         105.0       1.9
         106.0      60.5
         107.0     100.0
         108.0       8.0
         116.0       1.9
         117.0       1.9
         121.0       2.2
         123.0       4.1
         124.0       8.6
         125.0       1.0
         126.0       1.0
         127.0       3.2
         128.0       2.7
         131.0       1.6
         132.0       4.8
         133.0       4.9
         148.0      10.3
         149.0      25.0
         150.0       9.2
         151.0       1.9
         221.0       3.6
         222.0      13.3
         223.0       6.7
         224.0       1.1
         239.0       1.0
         255.0       4.3
         256.0      35.0
         257.0       6.8
         258.0       2.2
    

90 MHz in DMSO-d6

400 MHz in DMSO-d6


  • 1H NMR 89.56 MHz
    C15 H16 N2 S 0.036 g : 0.5 ml DMSO-d6
    1,3-di(p-tolyl)-2-thiourea
    ChemicalStructure
        Assign.     Shift(ppm)
    A 9.57 B 7.327 C 7.131 D 2.274 J(B,C)=8.5HZ

         Hz     ppm     Int.
    

        857.44   9.574    201
        662.13   7.394    223
        653.69   7.299    502
        641.56   7.164    430
        632.94   7.068    200
        203.75   2.276   1000
    


  • 1H NMR 399.65 MHz
    C15 H16 N2 S 0.039 g : 0.5 ml DMSO-d6
    1,3-di(p-tolyl)-2-thiourea
    ChemicalStructure
        Assign.     Shift(ppm)
    A 9.62 B 7.343 C 7.124 D 2.270

         Hz     ppm     Int.
    

       3843.69   9.618    260
       2939.45   7.356    347
       2931.06   7.335    414
       2850.95   7.134    369
       2842.56   7.113    307
        907.29   2.271   1000
    

KBr disc



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