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网站主页CAS数据库列表 619-56-7更多图谱4-氯苯甲酰胺(619-56-7)红外图谱(IR2)

4-氯苯甲酰胺

产品名称 4-氯苯甲酰胺

CAS号619-56-7

分子式C7H6ClNO

分子量155.58

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  • Mass

    MS-NW-0202          
    p-chlorobenzamide
    C7H6ClNO            (Mass of molecular ion:    155)
    

       Source Temperature: 180 °C
       Sample Temperature:   0 °C
       Direct, 75 eV
    

          16.0       3.8
          26.0       1.9
          27.0       2.5
          28.0       2.3
          35.0       1.2
          37.0       8.5
          37.5       1.2
          38.0      10.5
          39.0       4.5
          41.0       1.3
          43.0       2.1
          44.0      29.0
          46.0       1.6
          47.0       1.2
          49.0       6.2
          50.0      48.3
          51.0      22.1
          52.0       3.7
          53.0       2.4
          60.0       1.4
          61.0       3.9
          62.0       3.5
          63.0       4.5
          63.5       2.6
          64.0       1.5
          65.0       3.2
          72.0       1.6
          73.0       9.4
          74.0      34.7
          75.0      70.7
          76.0      20.2
          77.0       9.6
          84.0       3.8
          85.0       8.4
          86.0       1.8
          87.0       2.9
          90.0       1.0
          99.0       2.4
         101.0       1.0
         102.0       1.0
         103.0       1.8
         104.0       4.8
         109.0       1.4
         110.0       3.0
         111.0      69.1
         112.0       7.2
         113.0      22.9
         114.0       2.0
         126.0       1.0
         138.0       1.3
         139.0     100.0
         140.0       8.3
         141.0      31.9
         142.0       2.6
         155.0      56.3
         156.0       5.4
         157.0      18.8
         158.0       1.8
         173.0       1.7
         175.0       1.1
    

400 MHz in DMSO-d6

90 MHz in DMSO-d6


  • 1H NMR 399.65 MHz
    C7 H6 Cl N O 0.041 g : 0.5 ml DMSO-d6
    p-chlorobenzamide
    ChemicalStructure
        Assign.     Shift(ppm)
    A *1 8.11 B 7.935 C 7.546 D *1 7.54

         Hz     ppm     Int.
    

       3242.31   8.113    159
       3178.10   7.953    130
       3175.66   7.947    849
       3173.71   7.942    267
       3168.95   7.930    306
       3167.11   7.925    874
       3164.43   7.919    112
       3020.14   7.557   1000
       3018.19   7.553    323
       3013.43   7.541    415
       3011.72   7.536    946
    


  • 1H NMR 89.56 MHz
    C7 H6 Cl N O 0.039 g : 0.5 ml DMSO-d6
    p-chlorobenzamide
    ChemicalStructure
        Assign.     Shift(ppm)
    A *1 8.1 B 7.92 C 7.53 D *1 7.5 J(B,C)=8.6HZ

         Hz     ppm     Int.
    

        723.06   8.074    126
        716.63   8.002    147
        714.31   7.976    624
        712.38   7.955    227
        710.50   7.934     82
        707.75   7.903    325
        705.69   7.880    943
        703.44   7.855    164
        680.50   7.599    213
        678.44   7.576   1000
        676.44   7.553    312
        674.75   7.535    141
        671.69   7.500    365
        669.88   7.480    721
        668.00   7.459    164
        667.56   7.454    168
        665.13   7.427     79
        664.69   7.422     73
        663.94   7.414     63
    

KBr disc



nujol mull



4880 A,200 M,powder