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网站主页CAS数据库列表 609-66-5更多图谱2-氯苯甲酰胺(609-66-5)红外图谱(IR2)

2-氯苯甲酰胺

产品名称 2-氯苯甲酰胺

CAS号609-66-5

分子式C7H6ClNO

分子量155.58

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  • Mass

    MS-NW-1879          
    o-chlorobenzamide
    C7H6ClNO            (Mass of molecular ion:    155)
    

       Source Temperature: 170 °C
       Sample Temperature: 120 °C
       Direct, 75 eV
    

          18.0       2.0
          27.0       1.1
          28.0       1.5
          37.0       2.7
          37.5       1.0
          38.0       3.9
          39.0       2.4
          44.0      10.7
          45.5       1.3
          49.0       1.8
          50.0      15.6
          51.0       9.4
          52.0       1.3
          61.0       1.3
          63.0       1.6
          63.5       1.8
          65.0       1.8
          73.0       2.2
          74.0       7.9
          75.0      26.0
          76.0       7.9
          77.0       8.7
          84.0       1.4
          85.0       3.1
          87.0       1.0
          90.0       1.0
         102.0       1.4
         110.0       1.1
         111.0      37.7
         112.0       5.7
         113.0      12.3
         114.0       1.6
         137.0       1.1
         139.0     100.0
         140.0       7.6
         141.0      31.5
         142.0       2.6
         155.0      57.7
         156.0       4.6
         157.0      18.6
         158.0       1.5
    

400 MHz in CDCl3

90 MHz in CDCl3


  • 1H NMR 399.65 MHz
    C7 H6 Cl N O saturated in CDCl3
    o-chlorobenzamide
    ChemicalStructure
        Assign.     Shift(ppm)
    A 7.773 B 7.42 C 7.40 D 7.35 E *1 6.56 F *1 6.42 J(A,C)=1.4HZ. J(A,D)=7.6HZ.

         Hz     ppm     Int.
    

       3118.16   7.803     44
       3116.70   7.799     59
       3110.84   7.784    517
       3109.62   7.781    519
       3109.25   7.780    518
       3103.39   7.766    585
       3101.93   7.762    563
       3095.21   7.745     42
       2984.25   7.468     41
       2983.76   7.466     42
       2983.15   7.465     45
       2982.18   7.462     48
       2981.69   7.461     46
       2981.32   7.460     49
       2980.71   7.459     54
       2980.35   7.458     52
       2979.86   7.457     59
       2979.13   7.455     67
       2978.03   7.452     82
       2973.27   7.440    288
       2972.05   7.437    358
       2969.85   7.432    182
       2965.33   7.420    872
       2964.11   7.417   1000
       2961.43   7.411    523
       2961.06   7.410    528
       2955.69   7.396    657
       2953.98   7.392    631
       2948.00   7.377    348
       2946.17   7.372    358
       2943.12   7.365    495
       2941.41   7.360    445
       2935.79   7.346    544
       2934.20   7.342    517
       2928.59   7.328    238
       2927.12   7.325    212
       2923.83   7.316     65
       2923.34   7.315     62
       2922.97   7.314     56
       2921.02   7.309     45
       2919.92   7.307     45
       2622.56   6.563    136
       2564.21   6.417    132
    


  • 1H NMR 89.56 MHz
    C7 H6 Cl N O 0.038 g : 0.5 ml CDCl3
    o-chlorobenzamide
    ChemicalStructure
        Assign.     Shift(ppm)
    A 7.75 B 7.60 to 7.12 C 6.5

         Hz     ppm     Int.
    

        699.31   7.809    146
        698.75   7.803    157
        698.06   7.795    155
        697.31   7.786    140
        696.50   7.777    126
        694.56   7.756    217
        692.44   7.732    163
        691.38   7.720    190
        690.88   7.715    189
        690.56   7.711    186
        670.38   7.486     63
        669.94   7.481     74
        661.75   7.389   1000
        655.88   7.324    241
        655.56   7.320    242
        653.06   7.292    140
        652.56   7.287    146
        650.94   7.269    183
        583.94   6.521     86
    

in CDCl3



KBr disc



nujol mull



4880 A,200 M,powder