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MassMS-KW-0596 N-methyl-1-methylthio-2-nitrovinylamine C4H8N2O2S (Mass of molecular ion: 148)
Source Temperature: 240 °C Sample Temperature: 150 °C Reservoir, 75 eV
15.0 6.9 17.0 1.1 18.0 5.6 26.0 1.8 27.0 8.9 28.0 6.8 29.0 2.4 30.0 6.8 31.0 1.2 35.0 3.2 39.0 1.3 40.0 2.9 41.0 4.6 42.0 17.2 43.0 3.1 44.0 7.5 45.0 17.7 46.0 5.0 47.0 12.4 48.0 7.2 49.0 1.3 52.0 2.5 53.0 1.9 54.0 19.6 55.0 100.0 56.0 18.7 57.0 5.9 58.0 17.3 59.0 2.1 60.0 1.7 61.0 18.6 63.0 1.0 67.0 6.1 69.0 1.0 70.0 2.0 71.0 9.0 72.0 6.4 73.0 5.1 74.0 6.4 83.0 1.8 84.0 16.3 85.0 8.2 86.0 7.3 87.0 6.5 88.0 15.9 89.0 1.4 100.0 2.0 101.0 77.6 102.0 10.2 103.0 1.1 115.0 1.0 148.0 16.8 149.0 1.3
400 MHz in CDCl3
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1H NMR 399.65 MHz C4H8N2O2S 0.040 g : 0.5 ml CDCl3 N-methyl-1-methylthio-2-nitrovinylamine 
Assign. Shift(ppm)
A 10.5 B 6.616 C 3.146 D 2.468 double bond structure is uncertain
Hz ppm Int.4199.68 10.505 14 2740.18 6.855 2 2644.66 6.616 305 2547.46 6.373 2 1976.17 4.944 0 1554.42 3.889 2 1329.05 3.325 4 1323.70 3.312 4 1260.08 3.152 599 1254.74 3.139 577 1204.23 3.013 1 1199.04 3.000 1 1189.12 2.975 3 1183.78 2.962 4 1056.98 2.644 6 1014.56 2.538 1 986.49 2.468 1000 975.19 2.440 4 914.31 2.288 6 58.60 0.147 1
in CDCl3
KBr disk
Nujol
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