N-甲基-1-甲硫基-2-硝基乙烯胺

Mass

MS-KW-0596          
N-methyl-1-methylthio-2-nitrovinylamine
C4H8N2O2S           (Mass of molecular ion:    148)

   Source Temperature: 240 °C
   Sample Temperature: 150 °C
   Reservoir, 75 eV

      15.0       6.9
      17.0       1.1
      18.0       5.6
      26.0       1.8
      27.0       8.9
      28.0       6.8
      29.0       2.4
      30.0       6.8
      31.0       1.2
      35.0       3.2
      39.0       1.3
      40.0       2.9
      41.0       4.6
      42.0      17.2
      43.0       3.1
      44.0       7.5
      45.0      17.7
      46.0       5.0
      47.0      12.4
      48.0       7.2
      49.0       1.3
      52.0       2.5
      53.0       1.9
      54.0      19.6
      55.0     100.0
      56.0      18.7
      57.0       5.9
      58.0      17.3
      59.0       2.1
      60.0       1.7
      61.0      18.6
      63.0       1.0
      67.0       6.1
      69.0       1.0
      70.0       2.0
      71.0       9.0
      72.0       6.4
      73.0       5.1
      74.0       6.4
      83.0       1.8
      84.0      16.3
      85.0       8.2
      86.0       7.3
      87.0       6.5
      88.0      15.9
      89.0       1.4
     100.0       2.0
     101.0      77.6
     102.0      10.2
     103.0       1.1
     115.0       1.0
     148.0      16.8
     149.0       1.3

Assign. Shift(ppm) A 10.5 B 6.616 C 3.146 D 2.468 double bond structure is uncertain

     Hz     ppm     Int.

   4199.68  10.505     14
   2740.18   6.855      2
   2644.66   6.616    305
   2547.46   6.373      2
   1976.17   4.944      0
   1554.42   3.889      2
   1329.05   3.325      4
   1323.70   3.312      4
   1260.08   3.152    599
   1254.74   3.139    577
   1204.23   3.013      1
   1199.04   3.000      1
   1189.12   2.975      3
   1183.78   2.962      4
   1056.98   2.644      6
   1014.56   2.538      1
    986.49   2.468   1000
    975.19   2.440      4
    914.31   2.288      6
     58.60   0.147      1