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MS-NW-4368 2,3-dichloro-1-propanol C3H6Cl2O (Mass of molecular ion: 128)
Source Temperature: 230 °C Sample Temperature: 170 °C Reservoir, 75 eV
15.0 2.2 26.0 3.6 27.0 14.2 28.0 2.2 29.0 9.2 31.0 32.5 36.0 1.6 37.0 1.0 38.0 1.2 39.0 3.8 43.0 4.9 49.0 4.0 51.0 1.2 55.0 1.5 57.0 7.9 61.0 5.1 62.0 100.0 63.0 8.0 64.0 47.8 65.0 3.5 66.0 6.7 75.0 3.1 77.0 1.0 79.0 1.8 91.0 1.0 92.0 6.0 94.0 2.0 121.0 2.2
90 MHz in CDCl3
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1H NMR 89.56 MHz C3 H6 Cl2 O 0.04 ml : 0.5 ml CDCl3 2,3-dichloro-1-propanol Assign. Shift(ppm)
A 4.16 B *1 3.97 C *1 3.81 D 2.10
Hz ppm Int.
378.63 4.228 63 374.75 4.185 82 373.75 4.174 121 370.31 4.135 111 368.19 4.112 68 367.50 4.104 99 364.00 4.065 103 355.38 3.969 1000 351.31 3.923 440 350.75 3.917 406 344.00 3.842 746 337.81 3.772 460 337.06 3.764 422 187.88 2.098 432
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