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磷酸三(1,3-二氯异丙基)酯

CAS号13674-87-8

分子式C9H15Cl6O4P

分子量430.9

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  • Mass

    MS-NW-1628          
    tris(2-chloro-1-(chloromethyl)ethyl) phosphate
    C9H15Cl6O4P         (Mass of molecular ion:    428)
    

       Source Temperature: 210 °C
       Sample Temperature: 140 °C
       Direct, 75 eV
    

          15.0       2.9
          27.0       7.6
          28.0       1.2
          29.0       2.6
          31.0       3.9
          36.0       3.3
          38.0       1.3
          39.0      25.2
          40.0       3.2
          41.0      21.1
          42.0       1.7
          43.0       6.7
          44.0       1.5
          47.0       2.2
          49.0      28.4
          50.0       1.1
          51.0       8.9
          55.0       1.0
          57.0      12.5
          61.0       2.0
          62.0       1.9
          63.0       1.4
          65.0       1.7
          73.0       1.3
          74.0       1.0
          75.0     100.0
          76.0       5.9
          77.0      32.0
          78.0       2.3
          79.0       4.6
          81.0       6.7
          83.0       3.0
          85.0       1.6
          91.0       1.5
          93.0       1.9
          99.0      77.0
         109.0       1.3
         110.0       2.9
         111.0      12.4
         112.0       2.2
         113.0       7.7
         115.0       1.3
         117.0       4.2
         119.0       1.7
         123.0       2.0
         125.0       1.2
         135.0       1.4
         137.0       5.8
         141.0       1.0
         155.0      20.1
         157.0       6.6
         159.0      10.5
         161.0       3.4
         173.0       4.8
         175.0       1.8
         191.0      54.7
         192.0       2.0
         193.0      35.3
         194.0       1.3
         195.0       6.0
         209.0      37.0
         210.0       1.4
         211.0      24.6
         213.0       4.1
         233.0       1.3
         269.0       3.4
         271.0       3.4
         273.0       1.1
         301.0       6.5
         303.0       8.1
         305.0       3.6
         319.0      12.3
         321.0      16.1
         322.0       1.2
         323.0       8.3
         325.0       1.8
         379.0       9.3
         381.0      15.7
         382.0       1.4
         383.0      10.3
         385.0       2.8
    

90 MHz in CDCl3


  • 1H NMR 89.56 MHz
    C9 H15 Cl6 O4 P 0.031 g : 0.5 ml CDCl3
    tris(2-chloro-1-(chloromethyl)ethyl) phosphate
    ChemicalStructure
        Assign.     Shift(ppm)
    A 4.810 B 3.858 J(A,P-31)=8.1HZ

         Hz     ppm     Int.
    

        440.31   4.917     70
        437.25   4.883     38
        435.25   4.860    120
        432.19   4.826     83
        430.19   4.804     95
        427.13   4.770    115
        425.31   4.749     43
        422.06   4.713     84
        417.13   4.658     27
        348.00   3.886   1000
        342.88   3.829    864
    

in CDCl3



CCl4 solution



liquid film



4880 A,200 M,liquid