磷酸三(1,3-二氯异丙基)酯

Mass

MS-NW-1628          
tris(2-chloro-1-(chloromethyl)ethyl) phosphate
C9H15Cl6O4P         (Mass of molecular ion:    428)

   Source Temperature: 210 °C
   Sample Temperature: 140 °C
   Direct, 75 eV

      15.0       2.9
      27.0       7.6
      28.0       1.2
      29.0       2.6
      31.0       3.9
      36.0       3.3
      38.0       1.3
      39.0      25.2
      40.0       3.2
      41.0      21.1
      42.0       1.7
      43.0       6.7
      44.0       1.5
      47.0       2.2
      49.0      28.4
      50.0       1.1
      51.0       8.9
      55.0       1.0
      57.0      12.5
      61.0       2.0
      62.0       1.9
      63.0       1.4
      65.0       1.7
      73.0       1.3
      74.0       1.0
      75.0     100.0
      76.0       5.9
      77.0      32.0
      78.0       2.3
      79.0       4.6
      81.0       6.7
      83.0       3.0
      85.0       1.6
      91.0       1.5
      93.0       1.9
      99.0      77.0
     109.0       1.3
     110.0       2.9
     111.0      12.4
     112.0       2.2
     113.0       7.7
     115.0       1.3
     117.0       4.2
     119.0       1.7
     123.0       2.0
     125.0       1.2
     135.0       1.4
     137.0       5.8
     141.0       1.0
     155.0      20.1
     157.0       6.6
     159.0      10.5
     161.0       3.4
     173.0       4.8
     175.0       1.8
     191.0      54.7
     192.0       2.0
     193.0      35.3
     194.0       1.3
     195.0       6.0
     209.0      37.0
     210.0       1.4
     211.0      24.6
     213.0       4.1
     233.0       1.3
     269.0       3.4
     271.0       3.4
     273.0       1.1
     301.0       6.5
     303.0       8.1
     305.0       3.6
     319.0      12.3
     321.0      16.1
     322.0       1.2
     323.0       8.3
     325.0       1.8
     379.0       9.3
     381.0      15.7
     382.0       1.4
     383.0      10.3
     385.0       2.8

Assign. Shift(ppm) A 4.810 B 3.858 J(A,P-31)=8.1HZ

     Hz     ppm     Int.

    440.31   4.917     70
    437.25   4.883     38
    435.25   4.860    120
    432.19   4.826     83
    430.19   4.804     95
    427.13   4.770    115
    425.31   4.749     43
    422.06   4.713     84
    417.13   4.658     27
    348.00   3.886   1000
    342.88   3.829    864