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MassMS-IW-4236 7-nitroquinoline C9H6N2O2 (Mass of molecular ion: 174)
Source Temperature: 230 °C Sample Temperature: 150 °C Reservoir, 75 eV
28.0 1.4 30.0 1.4 39.0 1.6 50.0 3.8 51.0 7.9 52.0 1.2 62.0 1.6 63.0 3.4 74.0 4.3 75.0 11.4 76.0 3.3 77.0 15.5 78.0 1.7 89.0 4.6 99.0 1.3 100.0 3.2 101.0 35.9 102.0 10.6 116.0 20.8 117.0 2.3 127.0 4.8 128.0 88.8 129.0 9.3 144.0 4.4 174.0 100.0 175.0 11.0
parameter in acetone
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1H NMR 300 MHz C9 H6 N2 O2 0.050 g : 1 ml acetone 7-nitroquinoline 
Parameter ppm Hz
D(A) 9.094 D(B) 7.717 D(C) 8.495 D(D) 8.208 D(E) 8.321 D(F) 8.836 J(A,B) 4.27 J(A,C) 1.78 J(A,D) 0.0 J(A,E) 0.0 J(A,F) 0.0 J(B,C) 8.41 J(B,D) 0.0 J(B,E) 0.0 J(B,F) 0.0 J(C,D) 0.0 J(C,E) 0.0 J(C,F) 0.5 J(D,E) 8.99 J(D,F) 0.5 J(E,F) 2.33 BLACK,P.J. & HEFFERNAN,M.L. AUST.J.CHEM. 17, 558 (1964)
Hz ppm Int.2731.23 9.104 598 2729.47 9.098 619 2726.97 9.090 621 2725.21 9.084 621 2651.96 8.840 801 2649.67 8.832 820 2553.51 8.512 427 2552.06 8.507 422 2545.08 8.484 455 2543.65 8.479 452 2502.52 8.342 454 2500.24 8.334 434 2493.54 8.312 754 2491.25 8.304 741 2466.49 8.222 999 2466.14 8.220 1000 2457.52 8.192 589 2457.15 8.190 584 2321.35 7.738 611 2317.08 7.724 603 2312.96 7.710 573 2308.68 7.696 558
KBr disc
nujol mull
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