邻碘苯甲酰氯

产品名称邻碘苯甲酰氯

CAS号609-67-6

分子式C7H4ClIO

分子量266.46

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¹HNMR

IR1

Mass

MS-IW-3828          
o-iodobenzoyl chloride
C7H4ClIO            (Mass of molecular ion:    266)

   Source Temperature: 220 °C
   Sample Temperature: 150 °C
   Reservoir, 75 eV

      49.0       1.0
      50.0      10.0
      73.0       1.1
      74.0       5.2
      75.0       6.8
      76.0      20.2
      77.0       1.7
     104.0       2.7
     111.0       2.0
     115.5       3.4
     127.0       2.8
     203.0      24.3
     204.0       1.7
     231.0     100.0
     232.0       7.8
     266.0      13.3
     267.0       1.0
     268.0       4.4

400 MHz in CDCl3

¹H NMR	399.65 MHz
C₇ H₄ Cl I O	0.040 g : 0.5 ml CDCl₃
o-iodobenzoyl chloride

    Assign.     Shift(ppm)

      A             8.080
      B             8.050
      C             7.505
      D             7.254

     Hz     ppm     Int.

   3234.50   8.094    739
   3234.13   8.093    750
   3232.79   8.090    805
   3226.20   8.073    850
   3224.85   8.070    870
   3221.80   8.062    838
   3220.95   8.060    960
   3216.55   8.049     57
   3214.23   8.043    865
   3213.87   8.042    903
   3213.01   8.040   1000
   3206.79   8.024     31
   3008.06   7.527    569
   3006.84   7.524    579
   3000.61   7.509    793
   3000.12   7.507    723
   2999.39   7.506    816
   2998.90   7.504    653
   2992.68   7.489    632
   2991.46   7.486    641
   2909.06   7.280     52
   2907.47   7.276    659
   2905.88   7.272    631
   2900.02   7.257    753
   2899.54   7.256    742
   2898.44   7.253    715
   2897.95   7.252    698
   2894.41   7.243     45
   2893.68   7.241     59
   2892.09   7.237    554
   2890.50   7.233    577

liquid film

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