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网站主页CAS数据库列表 606-37-1更多图谱1,3-二硝基萘(606-37-1)红外图谱(IR2)

1,3-二硝基萘

产品名称 1,3-二硝基萘

CAS号606-37-1

分子式C10H6N2O4

分子量218.17

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  • Mass

    MS-NW-8229          
    1,3-dinitronaphthalene
    C10H6N2O4           (Mass of molecular ion:    218)
    

       Source Temperature: 190 °C
       Sample Temperature: 120 °C
       Direct, 75 eV
    

          18.0       2.0
          28.0       3.7
          30.0      13.3
          39.0       4.5
          43.0       2.8
          50.0       9.0
          51.0       6.1
          52.0       2.9
          61.0       1.6
          62.0       5.0
          63.0      11.5
          64.0       2.3
          74.0      14.9
          75.0      15.2
          76.0      20.7
          77.0       4.9
          86.0       4.5
          87.0       8.6
          88.0       8.7
          89.0      12.6
          90.0       1.8
          95.0       6.0
          98.0       5.9
          99.0       8.2
         100.0       8.3
         101.0       5.4
         102.0      15.2
         103.0       1.5
         104.0       1.1
         105.0       2.1
         113.0      17.9
         114.0      48.7
         115.0       6.3
         116.0       6.4
         117.0       1.0
         122.0       1.4
         125.0      33.4
         126.0     100.0
         127.0      14.6
         128.0       3.5
         129.0       1.8
         130.0       9.2
         131.0       1.0
         140.0       1.3
         141.0      12.7
         142.0      14.6
         143.0       2.4
         144.0       4.8
         157.0       1.3
         158.0       1.2
         160.0       7.8
         161.0       1.1
         171.0      27.3
         172.0      24.1
         173.0       2.9
         188.0       4.0
         190.0       7.6
         201.0      63.7
         202.0       9.0
         203.0       1.0
         218.0      91.2
         219.0      10.8
         220.0       1.3
    

90 MHz in CDCl3


  • 1H NMR 89.56 MHz
    C10 H6 N2 O4 0.046 g : 0.5 ml CDCl3
    1,3-dinitronaphthalene
    ChemicalStructure
        Assign.     Shift(ppm)
    A 9.036 B 8.926 C 8.60 D 8.19 E *1 7.96 F *1 7.84 J(A,B)=2.2HZ.

         Hz     ppm     Int.
    

        813.25   9.081     40
        810.81   9.054    392
        810.31   9.048    401
        808.56   9.029    601
        808.00   9.022    582
        804.44   8.983     35
        803.88   8.976     33
        802.75   8.964     47
        800.31   8.937   1000
        798.06   8.911    702
        776.19   8.667    138
        775.50   8.660    253
        774.06   8.643    294
        773.19   8.634    277
        768.63   8.583    151
        767.06   8.565    228
        766.25   8.556    354
        765.63   8.549    381
        764.81   8.540    233
        739.69   8.260    221
        739.19   8.254    191
        738.56   8.247    203
        738.06   8.241    196
        737.06   8.230    176
        736.56   8.225    164
        735.13   8.209     41
        732.13   8.175    435
        730.13   8.153    394
        727.00   8.118     38
        726.44   8.112     39
        725.94   8.106     42
        725.56   8.102     42
        725.19   8.098     39
        724.31   8.088     60
        723.50   8.079     37
        723.00   8.073     38
        721.63   8.058    189
        719.81   8.038    310
        717.25   8.009     37
        716.06   7.996     47
        714.69   7.981    588
        712.88   7.960    428
        711.38   7.944    199
        708.25   7.909    491
        707.00   7.895    650
        706.06   7.884    620
        704.44   7.866    432
        701.31   7.831    204
        700.50   7.822    291
        699.00   7.805    353
        693.50   7.744    118
        692.06   7.728     96
    

in CDCl3



KBr disc



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