图谱信息 供应商 相关产品
网站主页CAS数据库列表 602-38-0更多图谱1,8-二硝基萘(602-38-0)核磁图(1HNMR)

1,8-二硝基萘

产品名称 1,8-二硝基萘

CAS号602-38-0

分子式C10H6N2O4

分子量218.17

展开


  • Mass

    MS-NW-0229          
    1,8-dinitronaphthalene
    C10H6N2O4           (Mass of molecular ion:    218)
    

       Source Temperature: 180 °C
       Sample Temperature:   0 °C
       Direct, 75 eV
    

          30.0       5.2
          38.0       1.2
          39.0       3.4
          50.0       6.7
          51.0       5.2
          52.0       1.2
          61.0       1.8
          62.0       6.7
          63.0      11.9
          64.0       4.1
          74.0      11.3
          75.0      11.8
          76.0       8.0
          77.0       3.1
          86.0       3.7
          87.0       6.5
          88.0      15.5
          89.0       6.2
          90.0       1.6
          98.0       4.1
          99.0       4.0
         100.0       3.6
         101.0       4.7
         102.0       8.6
         103.0       1.0
         104.0       1.9
         113.0      20.7
         114.0     100.0
         115.0      10.8
         116.0      11.7
         117.0       1.6
         119.0       3.5
         122.0       1.0
         125.0       1.3
         126.0      11.8
         127.0       2.7
         128.0       1.8
         129.0       1.0
         130.0       2.9
         132.0       1.7
         142.0      21.4
         143.0       2.5
         144.0       2.6
         158.0       2.0
         172.0      73.8
         173.0       9.3
         218.0      23.9
         219.0       2.7
    

400 MHz in DMSO-d6

90 MHz in CDCl3


  • 1H NMR 399.65 MHz
    C10 H6 N2 O4 0.038 g : 0.5 ml DMSO-d6
    1,8-dinitronaphthalene
    ChemicalStructure
        Assign.     Shift(ppm)
    A 8.586 B 8.504 C 7.940

         Hz     ppm     Int.
    

       3441.93   8.613     22
       3436.43   8.599    717
       3435.36   8.596    800
       3431.85   8.588     51
       3427.89   8.578    823
       3426.82   8.575    814
       3403.32   8.516    841
       3402.25   8.514    752
       3395.84   8.498    834
       3394.62   8.494    879
       3181.15   7.960    721
       3173.52   7.941    970
       3172.91   7.940   1000
       3165.44   7.921    628
    


  • 1H NMR 89.56 MHz
    C10 H6 N2 O4 0.042 g : 0.5 ml DMSO-d6
    1,8-dinitronaphthalene
    ChemicalStructure
        Assign.     Shift(ppm)
    A 8.57 B 8.50 C 7.938

         Hz     ppm     Int.
    

        773.25   8.634    359
        772.06   8.621    433
        767.94   8.575     40
        767.56   8.571     40
        764.94   8.542    849
        763.81   8.529   1000
        757.31   8.456    654
        756.13   8.443    474
        717.56   8.013    564
        709.69   7.925    690
        706.31   7.887     28
        705.75   7.881     26
        701.75   7.836    320
    

DMSO-d6



KBr disc



nujol mull



更多供应商