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MS-NW-8638 tetraethylgermane C8H20Ge (Mass of molecular ion: 190)
Source Temperature: 260 °C Sample Temperature: 130 °C Reservoir, 75 eV
26.0 1.0 27.0 5.0 28.0 1.7 29.0 3.7 70.0 3.8 71.0 7.4 72.0 5.1 73.0 15.3 74.0 9.4 75.0 18.6 76.0 3.3 77.0 10.6 79.0 1.7 85.0 1.7 87.0 2.9 88.0 1.5 89.0 3.8 91.0 1.6 97.0 2.2 99.0 12.6 100.0 2.8 101.0 43.2 102.0 7.2 103.0 54.3 104.0 13.8 105.0 51.4 106.0 1.7 107.0 10.1 128.0 1.3 129.0 57.4 130.0 4.6 131.0 76.9 132.0 26.9 133.0 100.0 134.0 5.0 135.0 21.0 157.0 39.4 158.0 2.8 159.0 52.0 160.0 18.3 161.0 69.5 162.0 4.6 163.0 14.5 164.0 1.0 188.0 1.1 190.0 1.5 207.0 1.4
400 MHz in CDCl3
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1H NMR 399.65 MHz C8 H20 Ge 0.05 ml : 0.5 ml CDCl3 tetraethylgermane Assign. Shift(ppm)
A 1.013 B 0.710
Hz ppm Int.
430.42 1.077 24 413.57 1.035 508 413.09 1.034 621 405.40 1.015 920 404.79 1.013 1000 397.09 0.994 674 396.61 0.993 556 294.92 0.738 314 294.19 0.737 316 286.99 0.719 712 286.13 0.716 479 278.93 0.698 617 271.12 0.679 213 270.39 0.677 228
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