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MassMS-NW-8005 chlorotriphenylgermane C18H15ClGe (Mass of molecular ion: 340)
Source Temperature: 160 °C Sample Temperature: 100 °C Direct, 75 eV
18.0 2.2 27.0 1.0 50.0 2.5 51.0 14.9 52.0 1.1 77.0 22.4 78.0 2.1 95.0 1.0 97.0 1.3 99.0 1.8 105.0 5.6 107.0 9.1 108.0 2.1 109.0 11.8 111.0 5.2 121.0 1.0 123.0 1.3 125.0 1.4 147.0 7.5 149.0 9.7 150.0 3.8 151.0 12.5 152.0 4.9 153.0 3.5 154.0 100.0 155.0 13.1 223.0 1.2 224.0 1.3 225.0 1.8 226.0 2.1 227.0 2.0 228.0 1.0 259.0 19.6 260.0 2.8 261.0 31.8 262.0 11.5 263.0 43.3 264.0 8.0 265.0 18.6 266.0 2.5 267.0 2.5 301.0 1.6 303.0 2.0 304.0 1.0 305.0 2.4 336.0 6.4 337.0 1.4 338.0 10.4 339.0 4.6 340.0 14.0 341.0 3.6 342.0 6.4 343.0 1.2
400 MHz in CDCl3
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1H NMR 399.65 MHz C18 H15 Cl Ge 0.030 g : 0.5 ml CDCl3 chlorotriphenylgermane 
Assign. Shift(ppm)
A 7.637 B 7.46 C 7.43
Hz ppm Int.3058.72 7.654 95 3056.64 7.649 627 3055.05 7.645 807 3053.83 7.642 403 3051.03 7.635 297 3049.07 7.630 771 3047.12 7.625 834 2995.61 7.496 49 2994.02 7.492 102 2992.43 7.488 79 2991.09 7.485 67 2986.94 7.474 311 2986.21 7.473 336 2983.52 7.466 195 2981.69 7.461 420 2979.98 7.457 808 2978.03 7.452 1000 2976.44 7.448 481 2973.27 7.440 315 2972.17 7.437 474 2970.83 7.434 715 2969.24 7.430 247 2965.94 7.422 150 2964.60 7.418 264 2963.62 7.416 145 2962.04 7.412 180
in CDCl3
KBr disc
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