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网站主页CAS数据库列表 59641-25-7更多图谱2-氯-3-吡咯烷-1,4-萘醌(59641-25-7)核磁图(1HNMR)

2-氯-3-吡咯烷-1,4-萘醌

产品名称 2-氯-3-吡咯烷-1,4-萘醌

CAS号59641-25-7

分子式C14H12ClNO2

分子量261.7


  • Mass

    MS-NW-9910          
    2-chloro-3-(1-pyrrolidinyl)-1,4-naphthoquinone
    C14H12ClNO2         (Mass of molecular ion:    261)
    

       Source Temperature: 220 °C
       Sample Temperature: 140 °C
       Direct, 75 eV
    

          18.0       1.6
          27.0       1.2
          28.0       1.8
          39.0       1.6
          41.0       2.2
          42.0       1.4
          43.0       6.0
          50.0       1.7
          51.0       1.1
          55.0       1.4
          56.0       1.5
          68.0       1.7
          70.0      20.1
          71.0       1.1
          74.0       1.3
          75.0       2.3
          76.0       4.8
          77.0       2.1
          80.0       1.0
          87.0       1.5
          88.0       1.2
          89.0       1.3
          99.0       2.6
         101.0       3.5
         102.0       1.4
         104.0       3.4
         105.0       5.7
         109.5       1.5
         114.0       3.5
         115.0       3.1
         126.0       1.1
         128.0       1.6
         129.0       4.5
         130.0       1.3
         135.0       2.8
         136.0       1.1
         137.0       1.0
         142.0       1.0
         143.0       1.8
         149.0       1.1
         154.0       2.2
         157.0      17.3
         158.0       2.3
         163.0       2.1
         164.0       1.3
         167.0       1.2
         169.0       1.5
         170.0       3.7
         171.0       7.6
         172.0       4.5
         178.0       1.4
         180.0       1.2
         191.0       2.0
         192.0       5.0
         193.0       1.4
         194.0       1.8
         196.0       1.6
         197.0       2.9
         198.0      16.8
         199.0       2.9
         205.0       1.9
         206.0      13.3
         207.0       2.5
         208.0       5.3
         209.0       2.0
         210.0       1.2
         218.0       2.2
         219.0       1.6
         220.0       3.2
         222.0       1.3
         223.0       3.0
         224.0       3.4
         225.0       2.7
         226.0      17.4
         227.0       5.6
         228.0       3.2
         232.0       2.1
         233.0      17.9
         234.0       3.2
         235.0       5.9
         260.0      16.8
         261.0     100.0
         262.0      21.7
         263.0      34.6
         264.0       5.5
    

400 MHz in CDCl3


  • 1H NMR 399.65 MHz
    C14 H12 Cl N O2 0.036 g : 0.5 ml CDCl3
    2-chloro-3-(1-pyrrolidinyl)-1,4-naphthoquinone
    ChemicalStructure
        Assign.     Shift(ppm)
    A 8.078 B 7.904 C 7.670 D 7.587 E 3.970 F 1.934

         Hz     ppm     Int.
    

       3233.52   8.091    257
       3232.18   8.088    259
       3225.95   8.072    273
       3225.46   8.071    271
       3224.61   8.069    274
       3163.09   7.915    249
       3161.74   7.912    250
       3155.40   7.896    288
       3154.05   7.893    279
       3074.22   7.693    145
       3072.88   7.689    145
       3066.77   7.674    324
       3065.43   7.671    300
       3059.20   7.655    210
       3057.86   7.652    183
       3039.31   7.605    222
       3037.96   7.602    214
       3031.86   7.587    316
       3030.52   7.583    297
       3024.29   7.568    133
       3022.95   7.564    120
       1593.51   3.988    358
       1590.70   3.981    331
       1589.48   3.978    366
       1586.67   3.971    960
       1583.98   3.964    362
       1582.76   3.961    322
       1579.96   3.954    360
        785.16   1.965     48
        784.06   1.962     44
        779.91   1.952    379
        776.12   1.942    436
        773.07   1.935   1000
        770.14   1.928    432
        766.36   1.918    364
        762.21   1.908     49
        761.23   1.905     49
    

in CDCl3



KBr disc



nujol mull



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