二硝基苯

Mass

MS-IW-0830          
o-nitrobenzaldehyde tosylhydrazone
C14H13N3O4S         (Mass of molecular ion:    319)

   Source Temperature: 180 °C
   Sample Temperature: 210 °C
   Direct, 75 eV

      17.0       1.1
      18.0       6.2
      27.0       2.3
      28.0      11.4
      29.0       1.1
      30.0       4.3
      37.0       1.2
      38.0       2.5
      39.0      11.2
      40.0       1.1
      41.0       3.8
      44.0       4.3
      45.0       3.2
      48.0       2.2
      50.0       7.9
      51.0      34.7
      52.0      10.9
      53.0       2.0
      61.0       1.7
      62.0       4.7
      63.0      13.3
      64.0      15.7
      65.0      39.4
      66.0       3.5
      67.0       4.5
      69.0       1.1
      74.0       2.1
      75.0       2.2
      76.0       6.2
      77.0      35.9
      78.0      10.6
      79.0      13.4
      80.0       3.7
      85.0       1.0
      86.0       1.1
      87.0       1.1
      89.0       7.9
      90.0       5.1
      91.0     100.0
      92.0      58.3
      93.0       6.9
      95.0       1.2
     104.0       1.8
     105.0       6.1
     106.0       4.9
     107.0      12.2
     108.0       8.2
     109.0       1.4
     111.0       2.9
     119.0       2.9
     120.0       1.9
     121.0       3.8
     122.0       1.7
     123.0       3.3
     124.0       6.0
     135.0       7.7
     136.0       6.6
     137.0       1.5
     139.0      33.8
     140.0       6.7
     141.0       2.1
     155.0       1.6
     156.0      35.2
     157.0       3.6
     158.0       1.9
     163.0       9.0
     214.0       1.3

Assign. Shift(ppm) A 12.0 B 8.318 C 8.031 D 7.847 E 7.805 F 7.762 G 7.643 J 7.441 K 2.377

     Hz     ppm     Int.

   4773.87  11.946     96
   3324.29   8.319    465
   3214.57   8.044    170
   3213.66   8.042    174
   3206.33   8.023    195
   3205.41   8.021    187
   3141.85   7.862    115
   3140.39   7.858    125
   3133.98   7.842    190
   3132.51   7.839    184
   3125.74   7.822     71
   3123.72   7.817    379
   3122.07   7.813    140
   3117.13   7.800    150
   3115.48   7.796    431
   3110.17   7.783     91
   3109.43   7.781     93
   3102.84   7.764    155
   3102.11   7.763    147
   3101.56   7.761    147
   3094.96   7.745     79
   3094.23   7.743     76
   3093.68   7.741     69
   3062.54   7.664    116
   3061.08   7.660    125
   3055.22   7.645    117
   3054.48   7.643    140
   3053.75   7.642    134
   3053.02   7.640    128
   3047.16   7.625     86
   3045.51   7.621     83
   2978.65   7.454    284
   2977.92   7.452    325
   2970.04   7.432    297
   2969.31   7.430    261
    950.27   2.378   1000