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MassMS-IW-0830 o-nitrobenzaldehyde tosylhydrazone C14H13N3O4S (Mass of molecular ion: 319)
Source Temperature: 180 °C Sample Temperature: 210 °C Direct, 75 eV
17.0 1.1 18.0 6.2 27.0 2.3 28.0 11.4 29.0 1.1 30.0 4.3 37.0 1.2 38.0 2.5 39.0 11.2 40.0 1.1 41.0 3.8 44.0 4.3 45.0 3.2 48.0 2.2 50.0 7.9 51.0 34.7 52.0 10.9 53.0 2.0 61.0 1.7 62.0 4.7 63.0 13.3 64.0 15.7 65.0 39.4 66.0 3.5 67.0 4.5 69.0 1.1 74.0 2.1 75.0 2.2 76.0 6.2 77.0 35.9 78.0 10.6 79.0 13.4 80.0 3.7 85.0 1.0 86.0 1.1 87.0 1.1 89.0 7.9 90.0 5.1 91.0 100.0 92.0 58.3 93.0 6.9 95.0 1.2 104.0 1.8 105.0 6.1 106.0 4.9 107.0 12.2 108.0 8.2 109.0 1.4 111.0 2.9 119.0 2.9 120.0 1.9 121.0 3.8 122.0 1.7 123.0 3.3 124.0 6.0 135.0 7.7 136.0 6.6 137.0 1.5 139.0 33.8 140.0 6.7 141.0 2.1 155.0 1.6 156.0 35.2 157.0 3.6 158.0 1.9 163.0 9.0 214.0 1.3
400 MHz in DMSO-d6
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1H NMR 399.65 MHz C14 H13 N3 O4 S 0.038 g : 0.5 ml DMSO-d6 o-nitrobenzaldehyde tosylhydrazone 
Assign. Shift(ppm)
A 12.0 B 8.318 C 8.031 D 7.847 E 7.805 F 7.762 G 7.643 J 7.441 K 2.377
Hz ppm Int.4773.87 11.946 96 3324.29 8.319 465 3214.57 8.044 170 3213.66 8.042 174 3206.33 8.023 195 3205.41 8.021 187 3141.85 7.862 115 3140.39 7.858 125 3133.98 7.842 190 3132.51 7.839 184 3125.74 7.822 71 3123.72 7.817 379 3122.07 7.813 140 3117.13 7.800 150 3115.48 7.796 431 3110.17 7.783 91 3109.43 7.781 93 3102.84 7.764 155 3102.11 7.763 147 3101.56 7.761 147 3094.96 7.745 79 3094.23 7.743 76 3093.68 7.741 69 3062.54 7.664 116 3061.08 7.660 125 3055.22 7.645 117 3054.48 7.643 140 3053.75 7.642 134 3053.02 7.640 128 3047.16 7.625 86 3045.51 7.621 83 2978.65 7.454 284 2977.92 7.452 325 2970.04 7.432 297 2969.31 7.430 261 950.27 2.378 1000
in DMSO-d6
KBr disc
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