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MS-NW-3400 3'-methylacetophenone C9H10O (Mass of molecular ion: 134)
Source Temperature: 300 °C Sample Temperature: 190 °C Reservoir, 75 eV
15.0 1.9 27.0 1.5 38.0 1.8 39.0 10.0 41.0 2.4 43.0 11.7 50.0 3.5 51.0 5.9 52.0 1.3 61.0 1.3 62.0 3.4 63.0 8.5 64.0 2.3 65.0 18.9 66.0 1.2 74.0 1.5 75.0 1.0 77.0 2.5 89.0 7.0 90.0 3.8 91.0 80.9 92.0 7.0 105.0 1.0 119.0 100.0 120.0 9.0 134.0 37.2 135.0 3.7
90 MHz in CDCl3
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1H NMR 89.56 MHz C9 H10 O 0.04 ml : 0.5 ml CDCl3 3'-methylacetophenone Assign. Shift(ppm)
A 7.77 B 7.75 C 7.35 D 7.34 E 2.570 F 2.40
Hz ppm Int.
697.50 7.789 35 696.94 7.782 50 696.25 7.775 46 695.13 7.762 72 694.38 7.754 81 693.69 7.746 64 693.25 7.741 60 691.88 7.726 23 689.81 7.703 29 689.25 7.696 28 660.13 7.371 139 659.06 7.359 89 657.13 7.338 48 656.63 7.332 52 655.50 7.320 35 655.00 7.314 32 653.69 7.299 72 230.13 2.570 1000 228.63 2.553 38 214.63 2.397 374
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