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MS-NW-1489 3'-methoxyacetophenone C9H10O2 (Mass of molecular ion: 150)
Source Temperature: 250 °C Sample Temperature: 180 °C Reservoir, 75 eV
15.0 4.3 27.0 1.2 28.0 1.3 37.0 1.0 38.0 4.5 39.0 4.9 43.0 23.7 50.0 6.8 51.0 5.9 52.0 1.3 53.0 1.4 61.0 1.0 62.0 3.0 63.0 11.6 64.0 13.5 65.0 4.3 74.0 2.6 75.0 2.0 76.0 4.5 77.0 38.9 78.0 5.7 79.0 3.1 91.0 2.3 92.0 22.5 93.0 2.0 107.0 44.1 108.0 4.0 135.0 100.0 136.0 8.8 150.0 58.5 151.0 5.9
90 MHz in CDCl3
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1H NMR 89.56 MHz C9 H10 O2 0.04 ml : 0.5 ml CDCl3 3'-methoxyacetophenone Assign. Shift(ppm)
A 7.50 B 7.46 C 7.35 D 7.10 E 3.835 F 2.574
Hz ppm Int.
679.50 7.588 22 678.13 7.572 51 676.63 7.556 40 670.88 7.491 235 669.31 7.474 186 665.94 7.436 88 657.94 7.347 114 652.19 7.283 23 650.75 7.267 54 640.50 7.152 66 639.00 7.135 75 637.94 7.124 69 636.44 7.107 58 632.63 7.064 35 631.00 7.046 39 630.25 7.038 36 628.63 7.020 30 343.50 3.836 957 230.56 2.575 1000
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