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MS-NW-6407 3'-chloroacetophenone C8H7ClO (Mass of molecular ion: 154)
Source Temperature: 260 °C Sample Temperature: 190 °C Reservoir, 75 eV
15.0 3.9 18.0 1.1 37.0 1.6 38.0 2.7 39.0 2.0 42.0 1.2 43.0 31.5 49.0 1.2 50.0 10.7 51.0 6.0 55.5 1.1 61.0 1.6 62.0 1.3 63.0 2.3 69.5 1.7 73.0 1.8 74.0 5.3 75.0 19.9 76.0 5.8 77.0 3.2 85.0 2.7 89.0 1.7 111.0 48.7 112.0 4.9 113.0 15.8 114.0 1.5 139.0 100.0 140.0 8.2 141.0 33.0 142.0 2.7 154.0 34.7 155.0 3.4 156.0 11.3 157.0 1.0
90 MHz in CDCl3
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1H NMR 89.56 MHz C8 H7 Cl O 0.04 ml : 0.5 ml CDCl3 3'-chloroacetophenone Assign. Shift(ppm)
A 7.91 B 7.82 C 7.50 D 7.39 E 2.589
Hz ppm Int.
711.00 7.939 34 710.19 7.930 41 709.31 7.920 79 708.69 7.914 66 708.31 7.909 50 707.25 7.897 73 706.69 7.891 61 705.88 7.882 46 704.19 7.863 63 698.81 7.803 46 697.06 7.784 65 695.44 7.766 43 679.06 7.583 31 672.88 7.514 77 671.06 7.493 111 669.00 7.470 117 668.13 7.461 80 661.88 7.391 62 661.25 7.384 60 231.88 2.590 1000
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