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MS-NW-5468 2'-methoxyacetophenone C9H10O2 (Mass of molecular ion: 150)
Source Temperature: 260 °C Sample Temperature: 190 °C Reservoir, 75 eV
15.0 3.0 38.0 2.2 39.0 3.5 43.0 11.7 50.0 3.9 51.0 5.9 52.0 1.2 53.0 1.0 62.0 1.5 63.0 5.8 64.0 5.8 65.0 2.9 74.0 1.3 75.0 1.0 76.0 2.3 77.0 36.0 78.0 4.3 79.0 4.4 91.0 2.2 92.0 13.6 93.0 1.3 105.0 3.1 107.0 1.8 120.0 3.5 132.0 1.7 133.0 1.9 135.0 100.0 136.0 8.9 150.0 20.6 151.0 2.1
90 MHz in CDCl3
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1H NMR 89.56 MHz C9 H10 O2 0.05 ml : 0.5 ml CDCl3 2'-methoxyacetophenone Assign. Shift(ppm)
A 7.71 B 7.42 C 6.94 D 6.94 E 3.854 F 2.583
Hz ppm Int.
695.63 7.768 76 693.69 7.746 85 687.63 7.678 98 686.06 7.661 98 673.75 7.523 38 671.75 7.501 34 666.13 7.438 79 663.19 7.405 48 658.06 7.348 70 656.25 7.328 61 628.75 7.021 83 624.69 6.976 133 621.94 6.945 127 616.44 6.883 94 615.69 6.875 96 345.19 3.855 897 343.19 3.832 67 231.13 2.581 1000 227.13 2.537 29
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