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MassMS-NW-0753 o-methoxybenzaldehyde C8H8O2 (Mass of molecular ion: 136)
Source Temperature: 240 °C Sample Temperature: 150 °C Reservoir, 75 eV
15.0 2.1 17.0 2.9 18.0 14.2 27.0 1.8 28.0 13.1 29.0 3.9 31.0 2.0 32.0 3.2 37.0 2.8 38.0 6.7 39.0 18.1 49.0 1.1 50.0 12.7 51.0 15.3 52.0 2.7 53.0 3.5 61.0 2.2 62.0 5.1 63.0 14.8 64.0 11.1 65.0 22.0 66.0 1.7 74.0 5.3 75.0 4.0 76.0 29.4 77.0 56.3 78.0 23.0 79.0 17.2 80.0 1.8 81.0 1.0 89.0 1.7 90.0 14.7 91.0 14.0 92.0 22.2 93.0 7.5 94.0 7.8 104.0 22.3 105.0 17.9 106.0 1.6 107.0 13.1 108.0 2.3 109.0 2.1 118.0 25.1 119.0 27.4 120.0 6.9 121.0 14.7 122.0 1.4 124.0 1.7 135.0 53.9 136.0 100.0 137.0 9.0
90 MHz in CDCl3
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1H NMR 89.56 MHz C8 H8 O2 10.0 mol% in CDCl3 o-methoxybenzaldehyde 
Assign. Shift(ppm)
A 6.88 to 7.09 B 7.51 C 10.445 D 7.79 E 3.884
Hz ppm Int.935.81 10.449 275 935.00 10.440 242 703.13 7.851 113 701.31 7.831 89 700.88 7.826 85 695.06 7.761 115 693.69 7.746 104 693.25 7.741 99 682.63 7.623 61 680.69 7.601 57 675.19 7.539 87 674.31 7.530 87 673.63 7.522 63 672.06 7.505 79 666.94 7.447 118 665.00 7.426 98 633.63 7.075 54 632.63 7.064 88 631.81 7.055 88 627.88 7.011 95 626.81 6.999 128 625.63 6.986 113 624.88 6.978 91 624.44 6.973 61 623.88 6.967 30 619.31 6.916 66 618.56 6.907 116 617.88 6.900 98 616.75 6.887 34 347.81 3.884 1000
in CDCl3
CCl4 solution
liquid film
4880 A,200 M,liquid
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