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MassMS-NW-7800 5-quinolinol C9H7NO (Mass of molecular ion: 145)
Source Temperature: 160 °C Sample Temperature: 120 °C Direct, 75 eV
18.0 1.1 28.0 1.0 37.0 1.3 38.0 2.4 39.0 5.1 45.0 1.0 50.0 2.9 51.0 3.4 52.0 1.2 53.0 1.3 58.5 3.1 61.0 1.4 62.0 4.0 63.0 9.4 64.0 3.6 65.0 1.3 72.5 3.2 74.0 1.7 75.0 1.5 76.0 1.2 77.0 1.0 78.0 1.7 87.0 1.2 88.0 1.6 89.0 16.1 90.0 14.6 91.0 2.1 115.0 1.0 116.0 9.7 117.0 26.3 118.0 4.2 144.0 8.6 145.0 100.0 146.0 10.6
400 MHz in DMSO-d6
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1H NMR 399.65 MHz C9 H7 N O 0.018 g : 0.5 ml DMSO-d6 5-quinolinol 
Assign. Shift(ppm)
A 10.54 B 8.869 C 8.526 D 7.564 E 7.49 F 7.46 G 6.968 J(B,F)=4.2HZ. J(B,C)=1.8HZ. J(D,G)=7.5HZ. J(G,E)=1.1HZ.J(C,F)=8.4HZ.
Hz ppm Int.4210.63 10.536 1000 3547.75 8.878 422 3545.92 8.873 461 3543.54 8.867 448 3541.71 8.863 442 3412.94 8.540 268 3412.21 8.538 310 3411.29 8.536 321 3410.38 8.534 302 3404.52 8.519 279 3403.78 8.517 332 3402.87 8.515 315 3401.95 8.513 299 3032.14 7.587 314 3024.63 7.569 378 3023.71 7.566 575 3019.68 7.556 34 3018.77 7.554 38 3016.20 7.548 585 3002.83 7.514 32 2998.62 7.504 348 2997.70 7.501 575 2996.79 7.499 413 2993.67 7.491 52 2993.31 7.490 53 2992.94 7.489 53 2989.28 7.480 754 2985.25 7.470 469 2981.03 7.460 454 2978.47 7.453 56 2976.82 7.449 444 2974.26 7.443 40 2789.08 6.979 447 2787.98 6.977 468 2785.41 6.970 47 2784.50 6.968 44 2781.57 6.961 441 2780.47 6.958 434
in DMSO-d6
KBr disc
nujol mull
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