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MS-KW-0530 6-quinolinol C9H7NO (Mass of molecular ion: 145)
Source Temperature: 150 °C Sample Temperature: 120 °C Direct, 75 eV
38.0 1.4 39.0 2.9 50.0 1.4 51.0 1.7 52.0 1.1 53.0 1.1 59.0 1.3 62.0 2.5 63.0 6.6 64.0 2.4 72.5 4.0 89.0 10.3 90.0 10.8 91.0 1.5 116.0 6.7 117.0 11.6 118.0 4.2 119.0 1.4 144.0 5.6 145.0 100.0 146.0 10.4
400 MHz in DMSO-d6
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1H NMR 399.65 MHz C9H7NO 0.035 g : 0.5 ml DMSO-d6 6-quinolinol Assign. Shift(ppm)
A 10.05 B 8.673 C 8.144 D 7.886 E 7.406 F 7.338 G 7.167
Hz ppm Int.
4017.64 10.050 985 3466.95 8.673 834 3259.59 8.154 619 3251.65 8.134 629 3156.90 7.897 632 3148.20 7.875 660 2960.67 7.406 598 2937.47 7.348 637 2928.93 7.327 574 2865.15 7.167 1000
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