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网站主页CAS数据库列表 575-36-0更多图谱N-乙酰-1-萘胺(575-36-0)核磁图(13CNMR)

N-乙酰-1-萘胺

产品名称 N-乙酰-1-萘胺

CAS号575-36-0

分子式C12H11NO

分子量185.22

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  • Mass

    MS-NW-0410          
    1-acetamidonaphthalene
    C12H11NO            (Mass of molecular ion:    185)
    

       Source Temperature: 170 °C
       Sample Temperature: 130 °C
       Direct, 75 eV
    

          39.0       1.6
          43.0      10.0
          51.0       1.2
          62.0       1.1
          63.0       2.7
          65.0       1.2
          75.0       1.0
          88.0       1.1
          89.0       2.7
         113.0       1.4
         114.0       2.3
         115.0      21.8
         116.0       7.2
         117.0       1.1
         127.0       1.2
         140.0       2.2
         141.0       1.2
         142.0       2.9
         143.0     100.0
         144.0      12.8
         185.0      40.5
         186.0       5.6
    

400 MHz in DMSO-d6


  • 1H NMR 399.65 MHz
    C12 H11 N O 0.037 g : 0.5 ml DMSO-d6
    1-acetamidonaphthalene
    ChemicalStructure
        Assign.     Shift(ppm)
    A 9.96 B 8.110 C 7.926 D *1 7.75 E *1 7.72 F *2 7.56 G *2 7.52 J 7.489 K 2.209

         Hz     ppm     Int.
    

       3980.71   9.961    137
       3244.78   8.120    117
       3243.26   8.116    120
       3235.93   8.097    133
       3172.61   7.939    146
       3169.71   7.932     90
       3165.59   7.921    153
       3163.45   7.916    148
       3100.13   7.758    156
       3091.43   7.736    278
       3083.19   7.715    171
       3027.04   7.575     50
       3025.51   7.571     67
       3020.48   7.558    170
       3018.80   7.554    166
       3016.51   7.548    195
       3013.61   7.541    327
       3010.56   7.533    176
       3008.73   7.529    170
       3007.05   7.525    161
       3000.03   7.507    214
       2992.25   7.488    260
       2984.31   7.468    131
        883.18   2.210   1000
    

DMSO-d6



KBr disc



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