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网站主页CAS数据库列表 57-83-0更多图谱黄体酮(57-83-0)红外图谱(IR1)

黄体酮

产品名称 黄体酮

CAS号57-83-0

分子式C21H30O2

分子量314.46

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  • Mass

    MS2004-02325WA      
    progesterone
    C21H30O2            (Mass of molecular ion:    314)
    

       Source Temperature: 250 °C
       Sample Temperature:  35 °C
       Direct, 70 eV
    

          18.0       1.0
          27.0       1.4
          29.0       2.2
          39.0       2.8
          41.0      10.3
          43.0      40.5
          53.0       5.7
          55.0      10.8
          65.0       3.9
          66.0       1.5
          67.0      12.5
          68.0       1.6
          69.0       2.9
          71.0       8.1
          77.0      13.0
          78.0       3.2
          79.0      21.5
          80.0       3.2
          81.0      14.1
          82.0       1.4
          83.0       2.5
          84.0       6.1
          85.0       7.8
          86.0       1.1
          91.0      24.8
          92.0       4.3
          93.0      19.5
          94.0       7.1
          95.0      17.7
          96.0       3.0
          97.0       4.4
         100.5       1.3
         103.0       2.2
         104.0       1.5
         105.0      20.0
         106.0       5.5
         107.0      19.5
         108.0       5.3
         109.0      13.2
         110.0       3.3
         111.0       4.4
         115.0       3.3
         116.0       1.6
         117.0       7.2
         118.0       2.6
         119.0      13.9
         120.0       8.1
         121.0      15.4
         122.0      11.8
         123.0      16.7
         124.0     100.0
         125.0      12.1
         126.0       1.0
         128.0       2.6
         129.0       3.9
         130.0       1.9
         131.0      11.3
         132.0       6.9
         133.0      23.1
         134.0      12.3
         135.0      15.7
         136.0       7.9
         137.0      12.4
         138.0       4.2
         141.0       1.7
         142.0       1.4
         143.0       4.9
         144.0       2.7
         145.0      11.4
         146.0       5.2
         147.0      25.6
         148.0       8.2
         149.0      14.5
         150.0       3.0
         151.0       1.2
         155.0       2.6
         156.0       1.2
         157.0       4.8
         158.0       2.3
         159.0      11.6
         160.0       3.8
         161.0       7.2
         162.0       3.2
         163.0       4.8
         164.0       1.1
         169.0       1.9
         170.0       1.2
         171.0       5.1
         172.0       4.2
         173.0      15.8
         174.0       6.5
         175.0       6.0
         176.0       3.3
         177.0       4.7
         178.0       2.1
         183.0       2.3
         184.0       1.4
         185.0       5.7
         186.0       2.8
         187.0      14.0
         188.0       4.4
         189.0       3.8
         190.0      13.3
         191.0      27.4
         192.0       4.7
         193.0       1.4
         197.0       2.4
         198.0       1.2
         199.0       3.3
         200.0       2.3
         201.0       7.2
         202.0       4.1
         203.0       2.0
         205.0       1.0
         211.0       8.0
         212.0       2.3
         213.0       4.0
         214.0       3.0
         215.0       4.2
         216.0       3.0
         225.0       3.1
         226.0       2.6
         227.0       8.5
         228.0       5.5
         229.0      59.7
         230.0      14.3
         231.0       6.0
         232.0       1.9
         238.0       1.1
         239.0       3.2
         241.0       1.4
         243.0       4.4
         244.0      21.6
         245.0       4.0
         253.0       5.4
         254.0       5.1
         255.0       1.6
         256.0       3.4
         257.0       7.6
         258.0       2.2
         267.0       1.0
         269.0       1.2
         270.0       2.0
         271.0       7.8
         272.0      77.7
         273.0      15.8
         274.0       1.9
         281.0       3.2
         286.0       2.6
         296.0       7.3
         297.0       2.3
         299.0      12.4
         300.0       2.8
         314.0      87.5
         315.0      20.7
         316.0       3.0
    

400 MHz in CDCl3


  • 1H NMR 399.65 MHz
    C21 H30 O2 0.035 g : 0.5 ml CDCl3
    progesterone
    ChemicalStructure
        Assign.     Shift(ppm)
    A 5.737 B 2.544 C 2.40 D 2.47 to 2.33 E 2.289 F *2 2.187 G 2.130 J 2.07 K 2.05 L 1.870 M *1 1.71 N *2 1.69 P 1.65 Q 1.565 R 1.46 S 1.45 T *1 1.28 U 1.192 V 1.19 W 1.057 X 0.992 Y 0.670 ASSIGNED BY H-H AND C-H COSY.

         Hz     ppm     Int.
    

       2293.46   5.739    106
       2292.60   5.737    110
       2291.87   5.735    110
       1025.76   2.567     39
       1016.72   2.545     78
       1007.81   2.522     36
        977.05   2.445     32
        974.37   2.439     54
        972.05   2.433     39
        969.36   2.426     50
        964.60   2.414     33
        962.77   2.410     34
        960.08   2.403     77
        957.52   2.396     38
        955.08   2.390     55
        950.81   2.380     53
        949.71   2.377     48
        949.22   2.376     48
        947.51   2.371     48
        945.68   2.367     70
        943.85   2.362     43
        942.50   2.359     46
        941.77   2.357     42
        923.71   2.312     38
        921.14   2.305     43
        919.31   2.301     44
        916.87   2.295     40
        881.84   2.207     40
        879.88   2.202     40
        870.73   2.179     45
        869.02   2.175     39
        859.74   2.152     31
        856.81   2.144     33
        851.20   2.130   1000
        835.08   2.090     42
        832.15   2.083     45
        827.03   2.070     56
        824.22   2.063     67
        822.75   2.059     47
        819.34   2.051     32
        814.21   2.038     39
        811.04   2.030     42
        809.20   2.025     37
        755.98   1.892     30
        752.69   1.884     31
        739.75   1.851     31
        702.15   1.757     34
        697.14   1.745     36
        695.68   1.741     36
        688.60   1.724     65
        686.77   1.719     54
        683.11   1.710     84
        680.18   1.702     35
        677.49   1.696     55
        674.19   1.687     57
        669.07   1.675     47
        665.77   1.666     36
        663.94   1.662     34
        659.79   1.651     52
        658.33   1.648     33
        657.23   1.645     38
        654.79   1.639     32
        651.86   1.632     46
        650.39   1.628     39
        633.06   1.585     33
        629.52   1.576     30
        621.58   1.556     36
        618.16   1.547     32
        593.63   1.486     32
        591.31   1.480     33
        582.76   1.459     97
        578.86   1.449     30
        574.10   1.437     70
        499.27   1.250     44
        483.64   1.211     47
        476.68   1.193    622
        471.31   1.180     40
        466.67   1.168     36
        464.72   1.163     30
        407.96   1.021     31
        403.56   1.010     35
        395.87   0.991     30
        392.09   0.982     33
        267.70   0.670    673
    

in CDCl3



KBr disc



nujol mull