卡特缩合剂

Mass

MS-IW-6165          
((1-benzotriazolyl)oxy)tris(dimethylamino)phosphonium hexafluorophosphate
C12H22F6N6OP2       (Mass of molecular ion:    442)

   Source Temperature: 170 °C
   Sample Temperature: 180 °C
   Direct, 75 eV

      15.0       1.6
      18.0       5.0
      20.0       1.1
      28.0       4.6
      30.0       1.9
      37.0       2.7
      38.0       4.7
      39.0       4.5
      40.0       1.7
      41.0       7.1
      42.0      14.3
      43.0       6.9
      44.0      61.6
      44.5       1.9
      45.0      36.4
      45.5       2.7
      46.0       7.7
      47.0       1.8
      50.0       1.7
      51.0       2.4
      52.0       6.7
      57.0       1.8
      58.0       5.3
      59.5       1.2
      60.0       2.3
      61.0       1.8
      62.0       3.0
      63.0      15.4
      64.0      33.9
      65.0       7.9
      73.0       1.8
      75.0       1.5
      76.0       3.2
      77.0       3.4
      78.0       3.6
      88.0       3.2
      90.0       6.0
      91.0      64.2
      92.0      20.5
      93.0       5.7
     104.0       2.4
     107.0      11.2
     110.0       7.2
     111.0       1.0
     119.0     100.0
     120.0       9.7
     121.0      39.3
     122.0      17.9
     132.0       1.4
     133.0       7.7
     134.0      13.1
     135.0      92.3
     136.0      13.3
     138.0       2.2
     139.0       1.0
     153.0       4.0
     154.0       4.9
     165.0      25.4
     166.0       2.3
     176.0       1.7
     177.0      18.3
     178.0       7.9
     179.0      19.3
     180.0       4.8
     181.0       2.8
     182.0       2.7
     296.0       1.8

Assign. Shift(ppm) A 8.063 B 7.768 C 7.699 D 7.530 E 2.863

     Hz     ppm     Int.

   3226.93   8.075     49
   3219.24   8.056     32
   3218.38   8.053     53
   3105.59   7.771     32
   3104.74   7.769     30
   3098.75   7.754     34
   3097.78   7.752     32
   3080.93   7.710     35
   3080.08   7.707     58
   3079.10   7.705     35
   3071.66   7.686     35
   3009.40   7.531     32
   1149.78   2.877   1000
   1139.16   2.851    986