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N,N-二甲基-1,3-二氨基丙烷

产品名称 N,N-二甲基-1,3-二氨基丙烷

CAS号109-55-7

分子式C5H14N2

分子量102.18

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  • Mass

    MS-NW-0595          
    N,N-dimethyltrimethylenediamine
    C5H14N2             (Mass of molecular ion:    102)
    

       Source Temperature: 280 °C
       Sample Temperature: 170 °C
       Reservoir, 75 eV
    

          15.0       3.3
          17.0       1.5
          18.0       7.8
          27.0       1.6
          28.0       5.2
          29.0       2.0
          30.0      15.7
          41.0       2.4
          42.0      11.5
          43.0       4.7
          44.0      11.4
          45.0       2.5
          46.0       4.8
          56.0       5.9
          57.0       6.2
          58.0     100.0
          59.0       4.9
          70.0       3.9
          71.0       1.5
          72.0       6.2
          84.0       2.5
          85.0      20.4
          86.0       1.2
         102.0       2.9
    

90 MHz in CDCl3


  • 1H NMR 89.56 MHz
    C5 H14 N2 0.05 ml : 0.5 ml CDCl3
    N,N-dimethyltrimethylenediamine
    ChemicalStructure
        Assign.     Shift(ppm)
    A 2.745 B 2.25 C 2.216 D 1.60 E 1.15

         Hz     ppm     Int.
    

        252.63   2.821     56
        245.75   2.744    123
        238.88   2.668     74
        215.00   2.401     46
        214.31   2.393     46
        207.88   2.322     97
        204.75   2.287     34
        198.56   2.218   1000
        150.69   1.683     43
        150.00   1.675     48
        143.31   1.601     59
        136.63   1.526     30
        135.88   1.518     34
        103.00   1.151    140
    

in CDCl3



liquid film



4880 A,100M,liquid