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2,2,6,6-四氯环己醇

产品名称 2,2,6,6-四氯环己醇

CAS号56207-45-5

分子式C6H8Cl4O

分子量237.94


  • Mass

    MS-NW-7505          
    2,2,6,6-tetrachlorocyclohexanol
    C6H8Cl4O            (Mass of molecular ion:    236)
    

       Source Temperature: 260 °C
       Sample Temperature: 170 °C
       Reservoir, 75 eV
    

          18.0       1.3
          26.0       2.5
          27.0      14.2
          28.0       3.6
          29.0       8.3
          31.0       2.5
          35.0       1.2
          36.0       7.4
          37.0       1.3
          38.0       3.3
          39.0      22.2
          40.0       3.9
          41.0      19.9
          42.0       1.3
          43.0       1.5
          44.0       1.7
          47.0       1.7
          48.0       1.1
          49.0       4.5
          50.0       3.1
          51.0       5.5
          52.0       1.0
          53.0       2.6
          55.0       3.8
          57.0       3.7
          61.0       5.5
          62.0       1.6
          63.0       7.4
          64.0       1.0
          65.0      17.1
          66.0       2.1
          67.0       3.9
          69.0       2.7
          73.0       3.4
          74.0       1.1
          75.0      19.6
          76.0       4.9
          77.0       7.6
          78.0       3.5
          83.0       1.9
          85.0       1.7
          87.0       2.5
          89.0       2.4
          91.0     100.0
          92.0       3.8
          93.0      31.8
          94.0       1.5
          95.0       1.2
          96.0       3.4
          97.0       1.1
          98.0       2.2
          99.0       2.2
         101.0      24.8
         102.0       2.2
         103.0       9.5
         104.0       9.1
         105.0       2.6
         106.0       3.0
         109.0      11.8
         110.0      20.3
         111.0       9.1
         112.0      15.7
         113.0       2.2
         114.0       4.2
         117.0       1.2
         122.0      24.0
         123.0       2.2
         124.0      14.6
         125.0       4.7
         126.0       2.7
         127.0       2.6
         129.0       5.1
         130.0       1.1
         131.0       2.0
         135.0       3.4
         136.0      15.6
         137.0       6.9
         138.0      10.5
         139.0       3.9
         140.0       2.1
         143.0       1.6
         145.0       1.4
         147.0       2.3
         149.0       1.5
         165.0       4.9
         167.0       3.0
         169.0       4.0
         170.0       6.1
         171.0       3.7
         172.0       6.1
         173.0       1.6
         174.0       2.1
         183.0       8.2
         185.0       7.6
         187.0       2.8
         200.0       3.7
         201.0       6.3
         202.0       3.8
         203.0       5.8
         204.0       1.5
         205.0       2.0
         220.0       1.0
    

400 MHz in CDCl3


  • 1H NMR 399.65 MHz
    C6 H8 Cl4 O 0.040 g : 0.5 ml CDCl3
    2,2,6,6-tetrachlorocyclohexanol
    ChemicalStructure
        Assign.     Shift(ppm)
    A 4.186 B 3.18 C 2.797 D 2.361 E 2.009 F 1.756 J(A,B)=10.5HZ 90MHZ : HSP-06-093

         Hz     ppm     Int.
    

       1678.59   4.201    937
       1673.71   4.188     36
       1668.09   4.174    992
       1274.05   3.188   1000
       1269.53   3.177     35
       1269.17   3.176     35
       1268.55   3.175     34
       1263.55   3.162    950
       1129.64   2.827    325
       1128.05   2.823    318
       1126.34   2.819    547
       1123.17   2.811    354
       1122.19   2.808    243
       1114.87   2.790    407
       1113.04   2.786    440
       1111.69   2.782    647
       1109.62   2.777    357
       1108.40   2.774    395
       1102.66   2.760     44
       1101.44   2.757     40
       1100.83   2.755     40
        959.96   2.403    266
        958.98   2.400    260
        956.30   2.393    285
        955.32   2.391    266
        948.00   2.373    220
        946.66   2.369    488
        945.80   2.367    479
        944.58   2.364    406
        942.87   2.360    526
        942.14   2.358    492
        937.13   2.345     51
        936.89   2.345     51
        933.23   2.336    232
        932.13   2.333    329
        930.91   2.330    220
        929.44   2.326    252
        928.47   2.324    304
        927.25   2.321    200
        826.42   2.068     83
        823.49   2.061    158
        820.43   2.053     89
        813.96   2.037     85
        811.65   2.031    147
        810.30   2.028    275
        808.72   2.024    241
        806.76   2.019    113
        805.79   2.017    130
        799.19   2.000    127
        797.24   1.995    166
        795.53   1.991    343
        794.31   1.988    123
        793.21   1.985    127
        792.11   1.983    110
        785.40   1.966     89
        782.47   1.958    150
        779.42   1.951     78
        715.58   1.791    100
        711.91   1.782    318
        708.37   1.773    468
        704.71   1.764    329
        700.93   1.754    170
        697.27   1.745    267
        693.60   1.736    362
        689.94   1.727    243
        686.40   1.718     83
    

in CDCl3



KBr disc



nujol mull



4880 A,200 M,powder