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MS-NW-1060 1,5-dichloropentane C5H10Cl2 (Mass of molecular ion: 140)
Source Temperature: 240 °C Sample Temperature: 170 °C Reservoir, 75 eV
18.0 1.3 26.0 2.2 27.0 19.9 28.0 1.9 29.0 16.9 38.0 1.4 39.0 15.3 40.0 3.0 41.0 37.3 42.0 43.5 43.0 2.5 49.0 6.6 51.0 2.0 53.0 5.2 54.0 1.8 55.0 100.0 56.0 5.9 62.0 2.2 63.0 9.3 65.0 3.0 67.0 7.8 68.0 48.1 69.0 22.5 70.0 1.1 75.0 3.1 76.0 4.5 77.0 1.4 78.0 1.4 91.0 7.9 93.0 2.6 104.0 9.4 106.0 3.1
90 MHz in CDCl3
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1H NMR 89.56 MHz C5 H10 Cl2 0.02 ml : 0.5 ml CDCl3 1,5-dichloropentane Assign. Shift(ppm)
A 3.55 B 2.05 to 1.35
Hz ppm Int.
324.50 3.624 321 322.50 3.601 192 318.13 3.553 1000 311.81 3.482 511 169.00 1.888 189 163.19 1.823 307 161.94 1.809 328 159.38 1.780 184 157.19 1.756 370 156.06 1.743 372 154.50 1.726 223 151.94 1.697 360 151.44 1.691 357 149.13 1.666 219
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