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网站主页CAS数据库列表 5535-49-9更多图谱2-氯乙基苯基硫醚(5535-49-9)核磁图(13CNMR)

2-氯乙基苯基硫醚

产品名称 2-氯乙基苯基硫醚

CAS号5535-49-9

分子式C8H9ClS

分子量172.68

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  • Mass

    MS-IW-7364          
    (2-chloroethylthio)benzene
    C8H9ClS             (Mass of molecular ion:    172)
    

       Source Temperature: 230 °C
       Sample Temperature: 150 °C
       Reservoir, 75 eV
    

          27.0       3.4
          39.0       4.2
          45.0      24.1
          47.0       1.1
          50.0       2.3
          51.0       5.9
          58.0       1.2
          59.0       1.7
          63.0       2.5
          65.0       9.6
          66.0       4.1
          69.0       4.2
          77.0       6.1
          78.0       1.3
          79.0       4.1
          82.0       1.2
          84.0       1.3
          91.0       2.5
         108.0       2.6
         109.0      17.4
         110.0      16.3
         111.0       2.0
         123.0     100.0
         124.0       8.9
         125.0       5.1
         135.0       2.9
         136.0       1.2
         137.0       8.1
         172.0      53.3
         173.0       5.3
         174.0      19.7
         175.0       2.0
    

400 MHz in CDCl3


  • 1H NMR 399.65 MHz
    C8 H9 Cl S 0.05 ml : 0.5 ml CDCl3
    (2-chloroethylthio)benzene
    ChemicalStructure
        Assign.     Shift(ppm)
    A 7.368 B 7.288 C 7.221 D 3.583 E 3.192

         Hz     ppm     Int.
    

       2951.42   7.386    226
       2950.68   7.384    537
       2949.22   7.380    751
       2947.14   7.375    222
       2943.36   7.365    484
       2942.14   7.362    875
       2940.92   7.359    820
       2938.72   7.354    142
       2921.63   7.311    171
       2920.90   7.309    330
       2919.80   7.306    548
       2917.97   7.302    193
       2914.79   7.294    199
       2913.33   7.290    602
       2912.60   7.288   1000
       2911.13   7.285    462
       2906.49   7.273    289
       2905.15   7.270    503
       2902.71   7.264     93
       2892.70   7.239    265
       2891.24   7.235    466
       2889.89   7.232    258
       2886.23   7.222    182
       2883.91   7.217    504
       2881.59   7.211    127
       2878.05   7.202    109
       2876.71   7.199    181
       2875.49   7.196     94
       1440.43   3.605    776
       1436.52   3.595    167
       1433.47   3.587    597
       1432.74   3.585    723
       1430.79   3.581    499
       1427.86   3.573    177
       1424.44   3.565    909
       1283.45   3.212    897
       1279.91   3.203    173
       1276.86   3.195    505
       1275.39   3.192    707
       1274.29   3.189    548
       1271.24   3.181    158
       1267.46   3.172    752
       1265.14   3.166     40
    

in CDCl3



liquid film