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2-氯乙基-4-氯苯砜

产品名称 2-氯乙基-4-氯苯砜

CAS号16191-84-7

分子式C8H8Cl2O2S

分子量239.12

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  • Mass

    MS-IW-4921          
    2-chloroethyl p-chlorophenyl sulfone
    C8H8Cl2O2S          (Mass of molecular ion:    238)
    

       Source Temperature: 130 °C
       Sample Temperature: 110 °C
       Direct, 75 eV
    

          26.0       1.5
          27.0      20.8
          28.0       2.3
          36.0       3.9
          38.0       1.8
          39.0       1.1
          45.0       1.6
          49.0       1.0
          50.0      15.8
          51.0       8.4
          61.0       2.6
          62.0       1.3
          63.0      38.5
          64.0       1.4
          65.0      12.3
          69.0       1.3
          73.0       3.0
          74.0       9.3
          75.0      44.3
          76.0       9.7
          77.0       4.6
          84.0       1.2
          85.0       5.2
          87.0       2.2
          99.0       5.5
         101.0       2.1
         103.0       1.1
         108.0       1.6
         110.0       1.0
         111.0     100.0
         112.0      23.5
         113.0      37.5
         114.0       7.5
         115.0       1.0
         125.0       3.0
         127.0      15.1
         128.0       5.4
         129.0       4.9
         130.0       1.7
         131.0       3.7
         133.0       1.4
         138.0       1.2
         159.0      39.0
         160.0       3.2
         161.0      14.3
         162.0       1.1
         175.0      93.0
         176.0      14.6
         177.0      35.7
         178.0       5.3
         179.0       1.8
         190.0       1.8
         192.0       1.4
         202.0      10.0
         204.0       4.0
         210.0      31.9
         211.0       2.4
         212.0      21.7
         213.0       1.6
         214.0       4.3
         238.0      37.3
         239.0       3.7
         240.0      25.3
         241.0       2.4
         242.0       4.9
    

400 MHz in CDCl3


  • 1H NMR 399.65 MHz
    C8 H8 Cl2 O2 S 0.040 g : 0.5 ml CDCl3
    2-chloroethyl p-chlorophenyl sulfone
    ChemicalStructure
        Assign.     Shift(ppm)
    A 7.871 B 7.581 C 3.764 D 3.544

         Hz     ppm     Int.
    

       3152.95   7.890    127
       3150.63   7.884    843
       3148.56   7.879    298
       3143.80   7.867    332
       3141.72   7.862    948
       3139.40   7.856    138
       3036.25   7.598    163
       3033.81   7.592   1000
       3031.74   7.586    316
       3027.10   7.575    315
       3025.02   7.570    837
       3022.58   7.564    115
       3020.87   7.559     39
       1513.06   3.786    367
       1512.45   3.785    371
       1508.54   3.775    115
       1505.74   3.768    765
       1504.03   3.764    394
       1501.22   3.757    127
       1497.92   3.749    538
       1497.44   3.747    528
       1423.34   3.562    537
       1422.97   3.561    529
       1419.56   3.553    114
       1416.75   3.545    378
       1415.16   3.541    741
       1412.23   3.534    103
       1408.33   3.524    368
       1407.84   3.523    365
    

in CDCl3



KBr disc



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