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网站主页CAS数据库列表 5455-98-1更多图谱N-(2,3-环氧丙基)邻苯二甲酰胺(5455-98-1)质谱(MS)

N-(2,3-环氧丙基)邻苯二甲酰胺

产品名称 N-(2,3-环氧丙基)邻苯二甲酰胺

CAS号5455-98-1

分子式C11H9NO3

分子量203.19

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  • Mass

    MS-NW-6540          
    N-(2,3-epoxypropyl)phthalimide
    C11H9NO3            (Mass of molecular ion:    203)
    

       Source Temperature: 140 °C
       Sample Temperature: 110 °C
       Direct, 75 eV
    

          15.0       4.2
          17.0       1.0
          18.0       4.5
          26.0       1.5
          27.0       5.5
          28.0       2.7
          29.0       4.0
          31.0       2.7
          37.0       1.4
          38.0       2.9
          39.0       3.6
          40.0       1.4
          41.0       1.1
          42.0       2.1
          43.0       5.7
          49.0       1.2
          50.0      23.5
          51.0       9.5
          52.0       4.1
          53.0       1.0
          55.0       1.0
          56.0       1.8
          62.0       1.5
          63.0       3.0
          64.0       2.0
          65.0       1.0
          66.0       2.9
          70.0       2.3
          73.0       1.4
          74.0       8.9
          75.0      12.0
          76.0      41.9
          77.0      28.4
          78.0       3.0
          89.0       4.4
          90.0       6.0
          91.0       1.9
         102.0       7.6
         103.0       7.7
         104.0      33.0
         105.0      15.9
         106.0       1.9
         116.0       2.1
         117.0      12.5
         118.0       3.1
         119.0       1.1
         128.0       1.5
         129.0       3.6
         130.0      11.7
         131.0       1.5
         132.0       7.9
         133.0      14.8
         134.0       1.5
         144.0       1.5
         145.0      10.3
         146.0       9.8
         147.0       5.4
         148.0       1.3
         157.0       1.4
         159.0      28.3
         160.0     100.0
         161.0      52.3
         162.0       5.5
         172.0       2.4
         173.0       4.5
         174.0      12.4
         175.0       5.7
         185.0       5.5
         186.0       1.1
         203.0       7.4
         204.0       1.1
    

90 MHz in CDCl3


  • 1H NMR 89.56 MHz
    C11 H9 N O3 0.043 g : 0.5 ml CDCl3
    N-(2,3-epoxypropyl)phthalimide
    ChemicalStructure
        Assign.     Shift(ppm)
    A 7.85 B 7.75 C *1 3.95 D *1 3.81 E 3.238 F 2.80 G 2.690 J(C,D)=14.2HZ. J(F,G)=4.9HZ. J(E,G)=2.5HZ. J(E,F)=3.9HZ. J(C,E)=J(D,E)=4.9HZ.

         Hz     ppm     Int.
    

        709.88   7.927    359
        708.19   7.908     50
        707.19   7.897    225
        706.00   7.883    313
        705.19   7.874    284
        703.44   7.855    569
        701.31   7.831    877
        700.81   7.826   1000
        699.56   7.812    533
        697.50   7.789    393
        696.50   7.777    960
        696.00   7.772    987
        693.88   7.748    459
        692.81   7.736    112
        692.13   7.729    293
        691.31   7.719    329
        690.13   7.706    242
        687.38   7.676    378
        367.06   4.099     64
        362.00   4.042     78
        352.88   3.941    354
        350.19   3.911     49
        347.25   3.878    715
        344.63   3.849     55
        344.19   3.844     59
        342.31   3.823    596
        332.88   3.717     89
        328.00   3.663    126
        298.13   3.329    106
        295.63   3.301    118
        294.31   3.287    140
        293.31   3.276    145
        291.75   3.258    151
        290.69   3.246    160
        289.50   3.233    188
        288.19   3.218     94
        286.88   3.204    190
        285.69   3.190    102
        284.31   3.175    110
        281.75   3.146    103
        256.13   2.860    174
        255.69   2.855    173
        251.25   2.806    391
        250.88   2.802    390
        247.38   2.763    328
        247.00   2.758    323
        243.75   2.722    496
        241.19   2.694    468
        238.88   2.668    239
        236.31   2.639    202
    

in CDCl3



KBr disc



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