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MassMS-NW-6540 N-(2,3-epoxypropyl)phthalimide C11H9NO3 (Mass of molecular ion: 203)
Source Temperature: 140 °C Sample Temperature: 110 °C Direct, 75 eV
15.0 4.2 17.0 1.0 18.0 4.5 26.0 1.5 27.0 5.5 28.0 2.7 29.0 4.0 31.0 2.7 37.0 1.4 38.0 2.9 39.0 3.6 40.0 1.4 41.0 1.1 42.0 2.1 43.0 5.7 49.0 1.2 50.0 23.5 51.0 9.5 52.0 4.1 53.0 1.0 55.0 1.0 56.0 1.8 62.0 1.5 63.0 3.0 64.0 2.0 65.0 1.0 66.0 2.9 70.0 2.3 73.0 1.4 74.0 8.9 75.0 12.0 76.0 41.9 77.0 28.4 78.0 3.0 89.0 4.4 90.0 6.0 91.0 1.9 102.0 7.6 103.0 7.7 104.0 33.0 105.0 15.9 106.0 1.9 116.0 2.1 117.0 12.5 118.0 3.1 119.0 1.1 128.0 1.5 129.0 3.6 130.0 11.7 131.0 1.5 132.0 7.9 133.0 14.8 134.0 1.5 144.0 1.5 145.0 10.3 146.0 9.8 147.0 5.4 148.0 1.3 157.0 1.4 159.0 28.3 160.0 100.0 161.0 52.3 162.0 5.5 172.0 2.4 173.0 4.5 174.0 12.4 175.0 5.7 185.0 5.5 186.0 1.1 203.0 7.4 204.0 1.1
90 MHz in CDCl3
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1H NMR 89.56 MHz C11 H9 N O3 0.043 g : 0.5 ml CDCl3 N-(2,3-epoxypropyl)phthalimide 
Assign. Shift(ppm)
A 7.85 B 7.75 C *1 3.95 D *1 3.81 E 3.238 F 2.80 G 2.690 J(C,D)=14.2HZ. J(F,G)=4.9HZ. J(E,G)=2.5HZ. J(E,F)=3.9HZ. J(C,E)=J(D,E)=4.9HZ.
Hz ppm Int.709.88 7.927 359 708.19 7.908 50 707.19 7.897 225 706.00 7.883 313 705.19 7.874 284 703.44 7.855 569 701.31 7.831 877 700.81 7.826 1000 699.56 7.812 533 697.50 7.789 393 696.50 7.777 960 696.00 7.772 987 693.88 7.748 459 692.81 7.736 112 692.13 7.729 293 691.31 7.719 329 690.13 7.706 242 687.38 7.676 378 367.06 4.099 64 362.00 4.042 78 352.88 3.941 354 350.19 3.911 49 347.25 3.878 715 344.63 3.849 55 344.19 3.844 59 342.31 3.823 596 332.88 3.717 89 328.00 3.663 126 298.13 3.329 106 295.63 3.301 118 294.31 3.287 140 293.31 3.276 145 291.75 3.258 151 290.69 3.246 160 289.50 3.233 188 288.19 3.218 94 286.88 3.204 190 285.69 3.190 102 284.31 3.175 110 281.75 3.146 103 256.13 2.860 174 255.69 2.855 173 251.25 2.806 391 250.88 2.802 390 247.38 2.763 328 247.00 2.758 323 243.75 2.722 496 241.19 2.694 468 238.88 2.668 239 236.31 2.639 202
in CDCl3
KBr disc
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