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吲哚-3-乙酰肼

产品名称 吲哚-3-乙酰肼

CAS号5448-47-5

分子式C10H11N3O

分子量189.21

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  • Mass

    MS-NW-6678          
    3-indoleacetohydrazide
    C10H11N3O           (Mass of molecular ion:    189)
    

       Source Temperature: 200 °C
       Sample Temperature: 130 °C
       Direct, 75 eV
    

          18.0       3.8
          28.0       2.1
          31.0       3.1
          39.0       1.8
          50.0       2.7
          51.0       4.8
          52.0       2.3
          62.0       1.0
          63.0       2.5
          65.0       2.0
          74.0       2.0
          75.0       2.9
          76.0       3.6
          77.0      13.7
          78.0       1.7
         101.0       2.1
         102.0       7.0
         103.0      10.2
         104.0       1.3
         117.0       1.2
         128.0       4.1
         129.0       9.9
         130.0     100.0
         131.0      11.0
         144.0      17.6
         145.0       2.2
         146.0       1.0
         157.0       3.6
         158.0       3.4
         189.0      24.8
         190.0       3.3
    

400 MHz in DMSO-d6


  • 1H NMR 399.65 MHz
    C10 H11 N3 O 0.039 g : 0.5 ml DMSO-d6
    3-indoleacetohydrazide
    ChemicalStructure
        Assign.     Shift(ppm)
    A 10.9 B 9.15 C 7.579 D 7.338 E 7.187 F 7.062 G 6.974 J 4.21 K 3.464

         Hz     ppm     Int.
    

       4343.61  10.869    146
       3658.20   9.154    201
       3033.42   7.591    217
       3033.05   7.590    219
       3025.54   7.571    237
       3025.18   7.570    232
       2937.07   7.350    272
       2928.83   7.329    319
       2873.52   7.191    316
       2871.32   7.185    306
       2831.02   7.084    117
       2829.92   7.081    127
       2824.06   7.067    191
       2822.96   7.064    253
       2821.86   7.061    134
       2816.00   7.047    161
       2814.72   7.043    150
       2794.94   6.994    178
       2794.20   6.992    176
       2787.06   6.974    271
       2786.33   6.972    198
       2780.10   6.957    124
       2779.00   6.954    114
       1683.67   4.213    413
       1384.56   3.465   1000
    

in DMSO-d6



KBr disc



nujol mull



4880 A,200 M,powder